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Lipids Capsules Quality Standards
PAGE \* MERGEFORMAT 18
Lipids Capsules Quality Standards
【Abstract】 Objective To establish the lipid Capsule quality standards. Thin Layer Chromatography (TLC) of the system, fleece-flower root, hawthorn, cassia seed for qualitative identification, using high performance liquid chromatography (HPLC) system, fleece-flower root in the determination of 2,3,5,4 ‘ 4 2-Hydroxy-stilbene O β D glucoside content. The results of thin-layer chromatography for the test materials and control solution chromatography in the corresponding position of herbs, or reference substance chromatographic spots appear on the same color, and negative non-interference; HPLC in, 2,3,5,4 ‘ 4-hydroxy 2 Styrene 2 O β D Glucosidase in the range of 0 ~ 0.82 μg good linear relationship (r = 0.999 9), the average recovery was 97.4%. Conclusion TLC spots showing clear, specific, can be used for identification of lipid Capsule; high-performance liquid chromatography method is simple, rapid, high precision, accuracy, and can be used for drug quality control.
Keywords: lipid Capsule; thin-layer chromatography; high-performance liquid chromatography; 2,3,5,4 ‘ 4-hydroxy-stilbene 2 O β D Glucosidase
Quality Standard for Xuezhiling Capsules
Abstract: ObjectiveTo establish the quality standard for Xuezhiling Capsules. MethodsRadix polygoni, Multiflori preparata, Fructus crataegi, Semen cassiae were identified by TLC. The contents of 2,3,5,4 ‘ Tetrahydroxystilbene 2 O β D glucoside in Radix polygoni Multiflori preparata was determined by HPLC. ResultsSpots obtained from the test solutions had the same color in reference solution and medical material in the same location, and the blank solution had no interference. The linear range of albiflorin was from 0 to 0.82μg (r = 0.9999), the averge recovery was 97.4%. ConclusionIn TLC, the spots are very clear and specific to identify the herbal medicine in Xuezhiling Capsules. It is simple,
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