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Musk Bone Capsule TLC
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Musk Bone Capsule TLC
[Abstract] Objective To musk bone capsule of the TLC study. Methods TLC the other side of Dragon Blood, Chinese angelica, Chuanxiong, 37 for qualitative identification. The results of qualitative identification of the main features of drug TLC strong, with good reproducibility. Conclusion This method can be used as the varieties of quality standards for research.
[Keywords:] musk bone capsule thin-layer chromatography
Musk bone closed capsule is contained in the ‘Ministry of Health standards for traditional Chinese medicine set prescription pharmaceutical preparations’ No. 5 [1], from the red peony, Chinese angelica, 37, Chuanxiong, Dragon’s blood, nux vomica, etc. Chinese medicine composed of 22 Herbs. With scattered silt pain, continued reinforcement of the effectiveness of bone, in the clinic for bruises, muscle trauma fracture, congestion condensation, flash waist Chaqi. The current standard is only reproduces Strychnos, Dragon Blood, natural copper micro-identification, in order to better control its quality, this paper thin-layer chromatography prescriptions Dragon Blood, Chinese angelica, Chuanxiong, 37 and other herbs to identification.
A reagent and sample
Musk bone capsule (sample 1, sample 2, sample 3, respectively, for the three samples from different manufacturers); negative sample (homemade); dracorhodin perchlorate (Lot No. 110811 9302), Dragon’s blood control medicines (Lot No. 906 8803), Chinese angelica control medicines (Lot 927 9907), Chuanxiong control medicines (Lot 918 9001), ginsenoside Rg1 reference substance (Lot No. 110703 200424), 37 saponins R1 reference substance (Lot No. 110,745 -200,312) (reference substance in the control were purchased from Chinese medicinal drugs and biological products); silica gel G (Qingdao Marine Chemical Plant), the reagents were analytical pure.
2 Methods and Results
2.1 TLC Dragon’s Blood
[2,4] to take the contents of this product 6 g,
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