Rhinitis Shu water by TLC.docVIP

 PAGE \* MERGEFORMAT 7 Rhinitis Shu water by TLC [Abstract] Objective To establish rhinitis Shu water quality control methods. Methods TCL law, prescription mint, Angelica, Licorice for qualitative identification. The results in the TCL chromatography, the detection can mint, Angelica, Licorice. Conclusion The qualitative detection methods save time, fast, simple and can be used as the preparation of quality control methods. [Keywords:] Rhinitis Shu water were identified by TLC Rhinitis Shu water is from the skullcap, peppermint, Xanthium, Angelica, licorice, magnolia, etc. 9 Chinese herbal medicines, has a hot breeze, the role of the nasal awakened, mainly for acute and chronic rhinitis. Practice has proved that the drug is safe and results are obvious. This preparation is for external use medicine nasal drops superior to other oral agents, with the role of the rapid, non-first-pass effect of advantages. In order to effectively monitor the quality of their finished product, we are the main component of which mint, Angelica, Licorice carried out TLC. 1 Drugs and reagents Menthol, Imperatorin, glycyrrhetinic acid, were purchased from Chinese medicine and biological products; mint Mentha haplocalyx Briq.; Angelica Angelica dahurica (Fisch.ex Hoffm.) Benth.et Hook.f.; licorice Glycyrrhiza uralensis Fisch .; the above ingredients are commercially available; rhinitis Shu water from the Dalian Medical University Hospital to provide a (batch number20040305 specification of 5 ml / teams, each ml containing crude drug 1 g; silica gel G, Qingdao Ocean Chemical Factory Chupin; sodium carboxymethyl cellulose (CMC-Na), Shanghai chemical reagent company’s products. The reagents used were of analytical grade. 2 Methods and Results 2.1 mint by TLC [1] 2.1.1 Preparation of reference substance solution precision Weigh menthol standard, plus made from petroleum ether containing 2 mg per ml of solution, as a reference substance solution. 2.1.2 Preparat