Scutellaria Ju quality standard of clear solution_1.docVIP

 PAGE \* MERGEFORMAT 10 Scutellaria Ju quality standard of clear solution [Abstract] Objective To establish a clear solution Ju Scutellaria the quality control standards. Methods Identification by TLC preparation skullcap, wild chrysanthemum, using high performance liquid chromatography preparation of the content of baicalin. Results skullcap, wild chrysanthemum thin map spots were clear gaps without interference, baicalin 0.066 3 ~ 0.530 4 μg linear range, regression equation: Y = 3 × 100.7X +17 488 (R2 = 0.999 8), the average recovery was 98.39%, RSD = 0.90%. Conclusion The method is simple, accurate and reproducible solution for Scutellaria Ju Qing capsule quality control. [Keywords:] Scutellaria Ju Qing capsule solution, TLC; high performance liquid chromatography, mass standards; baicalin Abstract: Objective To establish the quality standard of Qinju Qingjie capsules. Methods Radix Scutellariae and Flos Chrysanthemi Indici were identified by TLC. The content of baicalin was determined by HPLC. Results The spots on TLC plates were clear without interference in the blank reference. The standard curve of baicalin was Y = 3 × 100.7X +17 488 (R2 = 0.999 8), linear range was 0.066 3 ~ 0.530 4 μg, average recovery rate of baicalin was 98.39%, RSD was 0.90%. Conclusion The method is simple, accurate , reproducible and can be used for the quality control of Qinju Qingjie capsules. Keywords:: Qinju Qingjie capsules, TLC, HPLC, quality standard; baicalin Scutellaria Ju Qing capsule by the solutions of our clinical experience were developed by the Chinese side six new drugs by the skullcap, wild chrysanthemum, licorice and other herbs Prescription 5 flavor is made with heat detoxification, clinically used for upper respiratory tract infections fever, sore throat and other significant effect. The test of its quality standards of the relevant content. An instrument and reagent High performance liquid chromatography (Waters510 pump, WaterU6K inject