Single drop liquid microextraction headspace analysis of traditional Chinese medicine in the high boiling point volatile compounds_0.docVIP

Single drop liquid microextraction headspace analysis of traditional Chinese medicine in the high boiling point volatile compounds_0.doc

  1. 1、本文档共14页,可阅读全部内容。
  2. 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
  3. 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载
  4. 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
  5. 5、该文档为VIP文档,如果想要下载,成为VIP会员后,下载免费。
  6. 6、成为VIP后,下载本文档将扣除1次下载权益。下载后,不支持退款、换文档。如有疑问请联系我们
  7. 7、成为VIP后,您将拥有八大权益,权益包括:VIP文档下载权益、阅读免打扰、文档格式转换、高级专利检索、专属身份标志、高级客服、多端互通、版权登记。
  8. 8、VIP文档为合作方或网友上传,每下载1次, 网站将根据用户上传文档的质量评分、类型等,对文档贡献者给予高额补贴、流量扶持。如果你也想贡献VIP文档。上传文档
查看更多
Single drop liquid microextraction headspace analysis of traditional Chinese medicine in the high boiling point volatile compounds_0

 PAGE \* MERGEFORMAT 14 Single drop liquid microextraction headspace analysis of traditional Chinese medicine in the high boiling point volatile compounds [Abstract] established the analysis of high boiling point volatile components of Chinese medicine in the ionic liquid headspace single-drop microextraction and liquid chromatography, and used fresh Zhu Li compound guaiacol solution of the content. The improved hanging drop device increases the droplet and micro injector tip contact area at the plastic casing, so that droplets of ionic liquid 12 μL, to improve the stability of the droplet and the sensitivity. investigate and optimize the factors affecting the extraction, determine the extraction conditions: the 12 μL 1-butyl-3-methylimidazolium hexafluorophosphate-based ([PF6]) as hanging drops in 5 mL containing 36% (w / V) NaCl in the sample solution, extraction temperature 80 ℃ , stirring speed 1000 r / min under the conditions of headspace extraction 30 min, extracted directly to the micro droplets sucked back into the injector, the HPLC. guaiacol in 0.05 ~ 1.6 mg / L a good linear relationship (r = 0.9997); the detection limit was 0.39 μg / L, guaiacol’s recovery was 97.6%, RSD 2.5%. This method is simple, accurate, sample preparation is simple, low cost, no pollution. [Keywords:] ionic liquid; Headspace single-drop microextraction; high boiling point volatile compounds; compound liquid fresh Zhu Li; guaiacol 1 Introduction Analysis of traditional Chinese medicine and its preparations often contain important activity of some volatile components, which require the use of certain methods of sample extraction and separation of pre-treatment and purification, and then chromatography. The traditional extraction method [1] solvent extraction, steam distillation, essential oil extraction and ultrasonic extraction method. There are also some new methods, such as headspace gas chromatography [2] and solid phase micro-extraction technique [3]. However,

您可能关注的文档

文档评论(0)

jiupshaieuk12 + 关注
实名认证
文档贡献者

该用户很懒,什么也没介绍

版权声明书
用户编号:6212135231000003

1亿VIP精品文档

相关文档