Pulsed Amperometry for Anti-fouling of Boron-doped Diamond in Electroanalysis of β-Agonists Application to Flow Injection for Pharmaceutical Analysis 英文参考文献.docVIP

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Pulsed Amperometry for Anti-fouling of Boron-doped Diamond in Electroanalysis of β-Agonists Application to Flow Injection for Pharmaceutical Analysis 英文参考文献.doc

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Pulsed Amperometry for Anti-fouling of Boron-doped Diamond in Electroanalysis of β-Agonists Application to Flow Injection for Pharmaceutical Analysis 英文参考文献

Sensors 2006, 6, 1837-1850 sensors ISSN 1424-8220 ? 2006 by MDPI /sensors Full Paper Pulsed Amperometry for Anti-fouling of Boron-doped Diamond in Electroanalysis of β-Agonists: Application to Flow Injection for Pharmaceutical Analysis Chanpen Karuwan 1,2, Thitirat Mantim 1,2, Patcharin Chaisuwan 1,2, Prapin Wilairat 1,2, Kate Grudpan 3, Piyada Jittangprasert 1,4, Yasuaki Einaga 5, Orawon Chailapakul 6, Leena Suntornsuk 7, Oraphan Anurukvorakun 7 and Duangjai Nacapricha 1,2,* 1 Flow Innovation-Research for Science and Technology Laboratories (FIRST Labs.), Faculty of Science, Mahidol University, Rama 6 Road, Bangkok, 10400 Thailand 2 Department of Chemistry, Faculty of Science, Mahidol University, Bangkok, Thailand 3 Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai, Thailand 4 Department of Chemistry, Faculty of Science, Srinakharinwirot University, Bangkok, Thailand 5 Department of Chemistry, Faculty of Science and Technology, Keio University, Japan 6 Department of Chemistry, Faculty of Science, Chulalongkorn University, Bangkok, Thailand 7 Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Mahidol University, Thailand * Author to whom correspondence should be addressed; E-mail: scdnc@mahidol.ac.th and dnacapricha@ Received: 1 August 2006 / Accepted: 14 December 2006 / Published: 26 December 2006 Abstract: This work presents the construction and application of boron-doped diamond (BDD) thin film electrode as sensor for the determination of three β-agonists, viz. salbutamol, terbutaline and clenbuterol. Although well-known as a chemically inert material, BDD film however shows fouling in detection of these compounds using fixed- potential mode amperometry. A suitable waveform for pulsed amperometric detection (PAD) was developed and used to determine the agonist compounds. It was seen that the developed PAD significantly refreshed the BDD surface for