中药棣棠花Kerria japonica化学成分的初步分析.pdfVIP

广东药学院学报 }ournal 0/ Guangdong Pharmaceutical University Oct. 20日，29(5) 中药楝棠花Kerriαjαporzicα 化学成分的初步 分析 孙彩云l ，柳鑫华1 ，王庆辉1 ，陆慧宁2 ，苏贤君3 ，张翠仙3 (1.河北理工大学轻工学院，河北唐山 063000; 2. 中山大学分析测试中心，广东广州 510275; 3. 广州中医药大学中药学院，广东广州 510006) 摘要:目的初步研究橡棠花挥发油的化学成分，为其进二步化学成分分析提供科学依据。方法首次对 云南、四川产橡棠花的干燥全草进行系统化学成分预试验;并采用水蒸气蒸悟法提取不同产地楝棠花挥 发泊，采用 GC-MS 对其化学成分进行分析。结果共得到 18 种化合物。其中 2-keto-6， 10 , 14-trimethyl- Pentadecanone 的相对质量分数最高，在四川禄棠花中达 39.19% ，而在云南橡棠花中高达 65.11% 。 结论所分析化合物首次从楝棠花精油中得到。 关键词:楝棠花;挥发油;GC-MS;化学成分 中图分类号:R284.1 文献标志码:A doi: 10. 3969/j. issn. 1006-8783.2013.05.011 文章编号:1006-8783(2013)05-0514-04 Research on chemical constituents and essential oil from Ken加japonica 1 1 1 3 3 SUN Caiyun ,LIU Xinhua ,WANG Qinghui ,LU Huinin矿，SU Xia时un ,ZHANG Cuixian ( 1. College 0/Light Industry ,Heibei Polytechnic University , r.αngshαn 063000 , China; 2. Center 0/Analysis and Measurement , Sun Yat-Sen University , Guangzhou 510275 , China; 3. School 0/ Chi时se Mα， terial Medicα ， Guangzhou University 0/ Chinese Medici肘， Guangzhou 510006 , China) Abstract; Objective To investigate the chemical constituents of volatile oil from Kerriα japonica. Methods Chemical constituents of Kerria japonica collected from Sichuan and Yunnan provinces were subjected to preliminarγexperiments ， and the chemical compositions of the essential oil extracted from them were also firstly analysed by GC-MS. Results 18 constituents of the volatìle oil from Kerria japonica in Sichuan and Yunnan provinces were identified. Moreover , the relative content of 2-keto-6 , 10 , 14-trimethyl-Pentadecanone was the highest in two kinds of Kerria japonicαfrom different origins ,and was 39. 19% in Kerria japonicαcollected from Sichuan province , while , was more than 65. 11 % in Kerria japonica collected