年产1万吨甲醇—水混合物系精馏工段工艺设计 大学论文.doc

毕业设计（论文）手册 课题名称：年产1万吨甲醇—水混合物系精馏工段 工艺设计 学 院： 石油化工学院 班 级： 生物工程1001班 学 号： 1032050110 姓 名： 陈博 指导教师： 姚秀清 2014 年 6 月 年产1万吨甲醇-水精馏工段工艺设计 陈博 （辽宁石油化工大学学院生物工程）99.5%；塔底残液的甲醇含量不大于0.5%）的基础上进行了物料衡算，确定相平衡方程和操作线方程；然后采用逐板计算法计算出了精馏塔的理论塔板数，由此得到实际塔板数32块，总的人孔数为3，塔径D=3.06m，塔高H=21.2m，以及冷凝器、再沸器及离心泵等附属设备的工艺参数，从而对这些设备进行了选型。最后绘制了相关的工艺流程图及精馏塔设备图。 关键词：甲醇；工艺设计；三塔精馏；常压塔 Process design of distillation of methanol-water system with an annual output of 10,000 tons chenbo (Liaoning University of Petroleum Chemical, Petroleum Institute of Chemical, Biological Engineering 1001, Yingkou, Liaoning, 115000) Abstract Because of the energy crisis and environmental pollution caused by fossil fuel combustion, it is very f necessary to find out the environmental friendly renewable energy. Methanol is not only an important chemical organic solvent, but also a potential new biofuels. In order to conform to the new national energy policy, it has the vital significance to use the renewable resources as energy After reading a lot of data, firstly, the design scheme of distillation section has been established. For contemporary biological methanol distillation process, No.3 of methanol column has especially been chosen to optimize design to refine crude methanol. The float valve tower has been selected as the tower equipment. Based on the related process parameters (including the material liquid handling capacity F=43.17kmol/h, feed temperature 70℃, with requirements for content of methanol in supertower product not less than 99.5%, content of the residual liquid n-butanol in the bottom tower less than 0.5%), the material balance has been done and the phase equilibrium equation and operating line equation have been established. Then using method of step-by-step calculation to calculate the theoretical plate number, the results are the actual number of plate Np=32, the total number of the manhole 3, tower diameter D