深冷处理对碳纤维介面性能的影响 - 华冈纺织期刊,journal of the hwa .pdfVIP

JHGT-22.3(152) (2015-09) Journal of the Hwa Gang Textile 華岡紡織期刊第二十二卷 第三期 ISSN 1025-9678 .tw/manuscript/pdf/jhgt-22.3(152)(2015).pdf 深冷處理對碳纖維介面性能的影響 Effect of ultralow temperature on the interfacial properties of Carbon fiber 1 1 1 1* 范王璽子 , 張蔭楠 , 邱夷平 , 許福軍 Wangxizi Fan, Yinnan Zhang, Yiping Qiu, Fujun Xu* 1 東華大學紡織學院上海納米紡織材料重點實驗室 Shanghai Key Laboratory of Advanced MicroNano Textile Materials, College of Textiles, Donghua University *許福軍: fjxu@ 摘要 文章採用深冷處理也稱為超低溫處理對聚丙烯腈基碳纖維進行介面改性。將處理前和處理後碳 纖維的介面性能進行對比研究。通過對碳纖維與環氧樹脂進行微滴實驗表明，深冷處理後碳纖 維的介面剪切強度（IFSS ）提高了29.5% 。原子力顯微鏡（AFM ）顯示處理後纖維表面變粗糙， 這與IFSS 的結果一致。採用和X 射線衍射(XRD)對碳纖維的結構進行表徵，結果表明處理後 纖維結構存在一些物理變化。 關鍵 字：深冷處理，碳纖維，介面改性 Abstract In this study, PAN-based carbon fiber was selected to undertaking bulk modification through ultralow temperature also called cryogenic treatment. The interfacial properties of un-treated and cryo-treated carbon fiber were studied in a comparative manner. The interfacial shear strength (IFSS) of modified carbon fibers with epoxy resin was characterized by means of the micro-bond test and the result showed an increase of 29.5%. The atomic force microscope (AFM) showed rougher surface after cryogenic treatment which in agreement with the result of IFSS. The structure of carbon fiber was characterized by X-ray Diffraction (XRD), which indicated some physical changes in fib