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chemical dosimetry during alpha irradiation a specific system for uv-vis in situ measurement在阿尔法化学剂量测定法原位紫外辐照一个特定的系统测量.pdf

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chemical dosimetry during alpha irradiation a specific system for uv-vis in situ measurement在阿尔法化学剂量测定法原位紫外辐照一个特定的系统测量

American Journal of Analytical Chemistry , 2012, 3, 6-11 /10.4236/ajac.2012.31002 Published Online January 2012 (http://www.SciRP.org/journal/ajac) Chemical Dosimetry during Alpha Irradiation: A Specific System for UV-Vis in Situ Measurement Cedric Costa, Johan Vandenborre, Francis Crumière, Guillaume Blain, Rachid Essehli, Massoud Fattahi Unité Mixte de Recherche 6457, École des Mines de Nantes Université de Nantes, Nantes, France Email: johan.vandenborre@subatech.in2p3.fr Received June 29, 2011; revised August 18, 2011; accepted September 2, 2011 ABSTRACT This paper is devoted to the study of the potentiality of the Fricke dosimeter for the characterization of the highly ener- getic (62.1 MeV) α particles beams generated by a new cyclotron facility, namely ARRONAX started in 2009. Such for this high energetic α beam, in situ dosimetry is performed in order to avoid radiation safety inconvenience and to earn run time of irradiation. Therefore, an in situ Fricke dosimetry protocol is developed and its reliability is checked by comparison with other experiments carried out by using the traditional method (ex situ Fricke dosimetry) within another cyclotron facility (CEMHTI) and by comparison with literature data. To author’s knowledge, it is the first time that Fricke dosimetry is performed during the α irradiation experiment. The results of these in situ dosimetry experiments show that the value of ferric ions radiolytic yield (G(Fe3+) = (11.7 ± 1.2) 10–7 mol·J–1) extrapolated from literature data can be used for this higher energy of α particles (Eα = 62.1 MeV). Keywords: In Situ UV-Vis Measurement; Chemical Dosimetry; High Energetic α Irradiation; Ferric Ion Radiolytic