原创力文档crystal growth and characterization of potassium manganese nickel sulphate hexahydrate—a new uv filter晶体生长和表征的硫酸镍锰钾hexahydrate-a新的紫外线过滤器.pdfVIP
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crystal growth and characterization of potassium manganese nickel sulphate hexahydrate—a new uv filter晶体生长和表征的硫酸镍锰钾hexahydrate-a新的紫外线过滤器
Journal of Minerals and Materials Characterization and Engineering, 2012, 11, 1121-1125
Published Online November 2012 (http://www.SciRP.org/journal/jmmce)
Crystal Growth and Characterization of Potassium
Manganese Nickel Sulphate Hexahydrate—
A New UV Filter
1 1 2
Vanitha Duraikkan , Sultan Asath Bahadur , Shunmuganarayanan Athimoolam
1Department of Physics, Kalasalingam University, Krishnankoil, India
2Department of Physics, University College of Engineering, Anna University of Technology, Thirunelveli, India
Email: vanithaklu@, s_a_bahadur@yahoo.co.in, athi81s@yahoo.co.in
Received July 17, 2012; revised August 22, 2012; accepted September 2, 2012
ABSTRACT
Potassium Manganese Nickel Sulphate Hexahydrate (KMNSH) crystals have been successfully grown by using tradi-
tional slow evaporation method. The empirical formula of KMNNSH is K Mn Ni (SO ) ·6H O with formula weight
2 0.1 0.9 4 2 2
430.7698. KMNNSH crystal revealed monoclinic space group P2(1)/c, a = 6.12(4) Å, b = 12.19(9) Å, c = 8.96(7) Å, α
= γ = 90˚, β = 105.3(2), V = 645(1)Å3, Z = 2, Dc = 2.2281 g/cm3 with deep green color. IR confirms that there is strong
interaction between free water molecules. The thermal analysis indicates that the water molecules are present in the
KMNNSH crystals. The transmission spectrometry of KMNNSH in the range from UV to near IR wavelengths is re-
ported. Atomic Absorption Spectroscopy also have been studied and discussed.
Keywords: Ultraviolet Filter; Potassium Manganese Nickel Sulphate; Tr
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