原创力文档dechlorination of trichloroethylene in groundwater by nanoscale bimetallic fepd particles地下水中三氯乙烯的脱氯纳米双金属fepd粒子.pdfVIP
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dechlorination of trichloroethylene in groundwater by nanoscale bimetallic fepd particles地下水中三氯乙烯的脱氯纳米双金属fepd粒子
J. Water Resource and Protection, 2009, 2, 78-83
doi:10.4236/jwarp.2009.12011 Published Online August 2009 (http://www.SciRP.org/journal/jwarp/).
Dechlorination of Trichloroethylene in Groundwater by
Nanoscale Bimetallic Fe/Pd Particles
1,2 1 1 1
Tielong LI , Shujing LI , Yongchao LI , Zhaohui JIN
1College of Environmental Science and Engineering, Nankai University, Tianjin, China
2 Tianjin Key Laboratory of Environmental Remediation and Pollution Control/Ministry of Education Key Laboratory of
Environmental Processes and Criteria, Nankai University, Tianjin, China
E-mail : litielong@
Received November 29, 2008; revised January 13, 2009; accepted February 14, 2009
Abstract
Palladium/iron bimetallic nanoparticles were synthesized using microemulsion method in the water-in-oil
(W/O) microemulsion system, which was made up of iso-octane, cetyltrimethyl-ammonium bromide
(CTAB), butanol and water and characterized by measuring the conductivity of the solution. Transmission
electron microscope (TEM) and energy dispersive X-ray microanalysis (EDX) analysis showed that the av-
erage diameter of synthesized palladium/iron bimetallic nanoparticles was less than 80 nm, which was much
smaller than the particles produced by the solution method. The palladium/iron bimetallic nanoscale particles
produced in the laboratory showed better performance on dechlorinating TCE than the other materials. The
nanoscale Fe/Pd particles exhibited high reactivity. When Pd content is 0.5%, the best TCE dechlorination
efficiency is achieved within 30min. And Fe/Pd nanoparticles show persistent reaction activity
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