原创力文档design and multicriteria optimization of a two-stage reactive extrusion process for the synthesis of thermoplastic polyurethanes设计和多准则优化两级反应挤出过程的热塑性聚氨酯的合成.pdfVIP
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design and multicriteria optimization of a two-stage reactive extrusion process for the synthesis of thermoplastic polyurethanes设计和多准则优化两级反应挤出过程的热塑性聚氨酯的合成
Engineering, 2012, 4, 497-514
/10.4236/eng.2012.49065 Published Online September 2012 (http://www.SciRP.org/journal/eng)
Design and Multicriteria Optimization of a Two-Stage
Reactive Extrusion Process for the Synthesis of
Thermoplastic Polyurethanes
1 1 2 1 1
Sandrine Hoppe , Dimitrios Meimaroglou , Mauricio Camargo , Christian Fonteix , Fernand Pla
1Laboratoire Réactions et Génie des Procédés (CNRS), Université de Lorraine, Nancy, France
2Equipe de Recherche des Processus Innovatifs (ENSGSI), Université de Lorraine, Nancy, France
Email: Fernand.Pla@univ-lorraine.fr, pla.fernand@hotmail.fr
Received June 23, 2012; revised July 20, 2012; accepted July 30, 2012
ABSTRACT
This paper presents the implementation of two multicriteria optimization methods based on different approaches,
namely, Rough Set Method (RSM) and Net Flow Method (NFM), to the manufacture by reactive extrusion of linear
Thermoplastic Polyurethanes (TPUs), appropriate for medical applications. A preliminary study allowed determining the
process operating conditions for which the polymerization time and the average residence time of the reactants in the
extruder are of the same order of magnitude. Prior to the optimization, a neural network model able to predict with ac-
ceptable accuracy the effect of the operating conditions on the output process variables, was constructed and validated.
This model was then used to determine, using Pareto’s concept, a set of non-dominated solutions constituting Pareto’s
domain. These solutions were then ranked according to the preferences of a decision maker using NFM and RSM. This
allowed providing the 10% highest ranked solut
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