determination of insecticide residues in vegetal fruits测定杀虫剂残留在蔬菜水果.pdfVIP

SAGE-Hindawi Access to Research Chromatography Research International Volume 2011, Article ID 713256, 6 pages doi:10.4061/2011/713256 Research Article Determination of Insecticide Residues in Vegetal Fruits Dasciana Rodrigues,1 Tecia Carvalho,2 Anayla Sousa,1 Vicente Sousa Neto,3 Pierre Fechine,1 and Ronaldo Nascimento1 1 Departamento de Qu´ımica Anal´ıtica e F´ısico Qu´ımica, Universidade Federal do Cear´a, Rua do Contorno, S/N Campus do Pici Bl 940 CEP, 60451-970 Fortaleza, CE, Brazil 2 Parque de Desenvolvimento Tecnol´ogico do Cear´a, Universidade Federal do Cear´a, Campus do Pici, CEP, 60457-970 Fortaleza, CE, Brazil 3 Departamento de Engenharia Hidr´aulica e Saneamento, Universidade Federal do Cear´a, Rua do Contorno, S/N Campus do Pici Bl 713 CEP, 60451-970 Fortaleza, CE, Brazil Correspondence should be addressed to Ronaldo Nascimento, ronaldo@ufc.br Received 4 November 2010; Accepted 23 December 2010 Academic Editor: Esther Turiel Copyright © 2011 Dasciana Rodrigues et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Pesticides compounds represent an important class of pollutants for food, soil and surface water resources. Thus, a simplified ´ method using gas chromatography was used for determining five insecticide residues in fruit samples produced in Ceara State (Brazil). The insecticides were simultaneously extracted from the fruit samples with a mixture of water-methanol (1 : 1 %v/v) from lipid-containing crops and th