原创力文档effect of different calcination process and gd2o3 as impurities on the different phases of bi-based superconductor影响不同的煅烧过程和gd2o3 bi-based超导体的杂质在不同阶段.pdfVIP
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effect of different calcination process and gd2o3 as impurities on the different phases of bi-based superconductor影响不同的煅烧过程和gd2o3 bi-based超导体的杂质在不同阶段
World Journal of Condensed Matter Physics, 2012, 2, 148-152
/10.4236/wjcmp.2012.23024 Published Online August 2012 (http://www.SciRP.org/journal/wjcmp)
Effect of Different Calcination Process and Gd O as
2 3
Impurities on the Different Phases of Bi-Based
Superconductor
1* 1 2 1
Ahmad Amirabadizadeh , Sara Memarzadeh , Naser Tajabor , Hadi Arabi
1Department of Physics, Faculty of Science, University of Birjand, Birjand, Iran; 2Department of Physics, Faculty of Science,
Ferdowsi University of Mashhad, Mashhad, Iran.
*
Email: ahmadamirabadi@
Received February 18th, 2012; revised March 25th, 2012; accepted April 3rd, 2012
ABSTRACT
In this research two samples of a nominal composition Bi Pb Sr Ca Cu O were prepared by the solid state reaction
1.6 0.4 2 2 3 x
method, using two different routes. Codes A and B are used to refer to the two samples. In preparing sample A, the
standard method for calcination was used, while for sample B, the SrCO and CaCO were calcinated at 1100˚C for 3 h.
3 3
Calcination was done separately on SrCO and CaCO in order to eliminate CO Then after mixing and grinding, the
3 3 2.
powder mixtures of Bi O , CuO, PbO, SrO and CaO were calcinated at 840˚C for 70 h. Also, the samples (samples C)
2 3
of nominal compositions Bi Pb Sr Ca Cu O + % x Gd O (% x = 0, 3, 5, 7 and 9) have been synthesized by this
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