原创力文档effect of ethylene carbonate (ec) plasticizer on poly (vinyl chloride)-liquid 50% epoxidised natural rubber (lenr50) based polymer electrolyte影响碳酸亚乙酯(ec)塑化剂对聚(氯乙烯)液体50% epoxidised天然橡胶(lenr50)为基础的聚合物电解质.pdfVIP
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effect of ethylene carbonate (ec) plasticizer on poly (vinyl chloride)-liquid 50% epoxidised natural rubber (lenr50) based polymer electrolyte影响碳酸亚乙酯(ec)塑化剂对聚(氯乙烯)液体50% epoxidised天然橡胶(lenr50)为基础的聚合物电解质
Materials Sciences and Application, 2011, 2, 818-826
doi:10.4236/msa.2011.27111 Published Online July 2011 (http://www.SciRP.org/journal/msa)
Effect of Ethylene Carbonate (EC) Plasticizer on
Poly (Vinyl Chloride)-Liquid 50% Epoxidised
Natural Rubber (LENR50) Based Polymer
Electrolyte
1* 2,3* 2,3 3 4
M. Y. A. Rahman , A. Ahmad , T. K. Lee , Y. Farina , H. M. Dahlan
1College of Engineering, University Tenaga Nasional, Kajang, Malaysia; 2Polymer Research Center, Faculty of Science and
Technology, Universiti Kebangsaan Malaysia, Bangi, Malaysia; 3School of Chemical Sciences and Food Technology, Faculty of
Science and Technology, Universiti Kebangsaan Malaysia, Bangi, Malaysia; 4Radiation Processing Technology Division, Malaysian
Nuclear Agency (MINT) Bangi, Kajang, Malaysia.
Email: yusri@.my, azizan@ukm.my.
Received April 14th, 2011; revised May 25th, 2011; accepted June 6th, 2011.
ABSTRACT
In this research, new thin film of a free standing electrolyte film containing poly(vinyl) chloride (PVC), 50% liquid
epoxidized natural rubber (LENR50), Ethylene carbonate (EC) blends as a host for the electrolyte which was doped
with lithium perchlorate (LiClO4) as the dopant salt was successfully prepared with solution casting technique. The
polymer electrolyte of PVC-LENR50-EC-LiClO 4 was characterized using impedance spectroscopy (EIS), scanning
electron microscopy (SEM) and Fourier transform infrared (ATR-FTIR). From the EIS results shows that electrolyte
exhibited the highest ionic conductivity of 2.1 × 10–7 Scm–1 at the 30 wt.% of LiClO . The ionic conductivity result was
4
supported by the morphological studies
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