preparation and physicochemical properties of the complex of naringenin with hydroxypropyl-β-cyclodextrin复杂的制备和物理化学性质与hydroxypropyl-β-cyclodextrin柚苷配基.pdfVIP

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preparation and physicochemical properties of the complex of naringenin with hydroxypropyl-β-cyclodextrin复杂的制备和物理化学性质与hydroxypropyl-β-cyclodextrin柚苷配基.pdf

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preparation and physicochemical properties of the complex of naringenin with hydroxypropyl-β-cyclodextrin复杂的制备和物理化学性质与hydroxypropyl-β-cyclodextrin柚苷配基

Molecules 2010, 15, 4401-4407; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Communication Preparation and Physicochemical Properties of the Complex of Naringenin with Hydroxypropyl-β-Cyclodextrin Jiping Wen 1, Benguo Liu 2, Erdong Yuan 3,*, Yuxiang Ma 1 and Yongyi Zhu 1 1 College of Grain and Food, Henan University of Technology, Zhengzhou 450052, China; E-Mails: wjp1380@163.com (J.W.); myx366@163.com (Y.M.); zyy4301@163.com (Y.Z.) 2 School of Food Science, Henan Institute of Science and Technology, Xinxiang 453003, China; E-Mail: zzgclbg@126.com (B.L.) 3 College of Light Industry and Food Science, South China University of Technology, Guangzhou 510640, China * Author to whom correspondence should be addressed; E-Mail: erdyuan@; Tel.: +86-20 Fax: +86-20 Received: 5 May 2010; in revised form: 7 June 2010 / Accepted: 9 June 2010 / Published: 18 June 2010 Abstract: In this study a complex of naringenin with hydroxypropyl-β-cyclodextrin (HP-β- CD) was prepared to improve the hydrophilicity of naringenin. The physicochemical properties of the complex were analyzed by ultraviolet-visible spectrometry (UV), infrared spectrometry (IR), X-ray diffractometry (XRD), differential scanning calorimetry (DSC). The result showed that naringenin had been molecularly dispersed in the HP-β-CD matrix, not forming a new compound and HPLC analysis showed that the solubility of naringenin in water was enhanced from 4.38 μg/mL to 1,272.31 μg/mL. Keywords: naringenin; hydroxypropyl-β-cyclodextrin; comp