工业分析（Industrial analysis）.docVIP

工业分析（Industrial analysis） 1. There are two main methods for the determination of ash in coal, namely slow ashing method and rapid ashing method. 2, in the coal ash determination experiment, removed from the furnace on the cupel, heat-resistant porcelain or asbestos net, cooling in air around 5min, into the dryer is cooled to room temperature (about 20min), weighing. 3. In the experiment of volatile determination of coal, a certain amount of air dried coal samples are taken and placed in the top of the cover. At the temperature of (900 + 10) C, the isolated air is heated by 7min. In order to reduce the mass fraction of the coal sample, the moisture content (Mad) of the coal sample was subtracted as the volatile yield. 2, using PAN as indicator, titrate immediately determination of aluminium in silicate by boiling with CuSO4 standard solution titration method, its purpose is to make the aluminum and EDTA coordination reaction was completed. 3. Whether the silicate sample can be decomposed by acid is mainly determined by the content of silica 4 and NaOH samples were decomposed by silver or platinum crucible, and the sample temperature was 650. 4. The common methods for the determination of moisture in coal are air drying and toluene distillation. 5. In toluene distillation, the moisture measuring tubes used are: range from 0 to 10, and the division value is 0.1. The moisture determination tube needs to be corrected and drawn a correction curve before it can be used. 6, the determination of total sulfur in coal, such as aldrin, coulometric titration and high temperature combustion neutralization method. 5. The determination methods of SiO2 in silicate sample are weight method and potassium fluosilicate volumetric method. 6, in the analysis of cement and its raw materials in the system, EDTA direct titration is Al titration after Fe3+ pH was adjusted to 1.8 to 2, and then with sulfosalicylic acid and as an indicator, the end point of titration solution from purple red co