响应面法优化亚麻籽油提取工艺.pdfVIP

※工艺技术 食品科学 2012, Vol. 33, No. 14 45 龙云飞，王沛佩，杨克迪，文衍宣 (广西大学化学化工学院，广西 南宁 530004) 为提高亚麻籽油的提取率，采用响应面法优化亚麻籽油的提取工艺条件。选取提取温度、提取时间、液 固比、搅拌速率作为影响因素，以正己烷为溶剂、亚麻籽油提取率为指标，在单因素试验的基础上，通过4 因 素 3 水平 Box-Behnken 试验，建立亚麻籽油提取率的二次多项式回归方程，经响应面回归分析得到优化组合条件。 结果表明：最佳提取工艺条件为提取温度 56 ℃、提取时间2.2h 、液固比 8:1(mL/g) 、搅拌速度310r/min 。在此条 件下亚麻籽油提取率为 98.12% ，与理论值98.28% 接近。结论：所得提取条件可靠。 亚麻籽；亚麻籽油；响应面法；提取工艺 Optimization of Extraction Process for Flaxseed Oil by Response Surface Analysis LONG Yun-fei ，WANG Pei-pei ，YANG Ke-di ，WEN Yan-xuan (College of Chemistry and Chemical Engineering, Guangxi University, Nanning 530004, China) Abstract ：In order to improve the extraction rate of flaxseed oil, response surface methodology was used to optimize the extraction conditions of flaxseed oil using n-hexane as the solvent. The effects of extraction temperature, extraction duration, solid- to-solvent ratio and stirring speed on the extraction rate of flaxseed oil were investigated by one-factor-at-a-time experiments. A quadratic polynomial regression model was fitted using a four-factor, three-level Box-Behnken design and analyzed using response surface methodology to obtain the optimal extraction conditions: temperature 56 ℃, solvent-to-solid ratio 8:1 (mL/g), stirring speed 310 r/min, and extraction time 2.2 h. Under these conditions, the extraction yield of flaxseed oil was 98.12%, closed to the theoretical value of 98.28%. In conclusion, the optimized extraction conditions are reliable. Key words ：flaxseed ；flaxseed oil ；response surface methodology ；extraction process 中图分类号：TS224.4 文献标识码：A 文章编号：1002-6630(2012)14-0045-05 亚麻籽又称胡麻籽，是亚麻科亚麻属的一年生或多 验以亚麻籽为原料、以正己烷作为溶剂