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超高效液相色谱-串联质谱法检测牛奶中双酚a determination of bisphenol a residues in milk by ultra performance liquid chromatography-tandem mass spectrometry
5 11 Vol. 5 No. 11
2014 11 Journal of Food Safety and Quality Nov. , 2014
-A
*
张建莹, 杨修斌, 罗 耀, 金晓蕾, 岳振峰 , 陈 波
( , 518045)
摘 要: 目的 A , A(bisphenol A, BPA)
-(ultra performance liquid chromatography-tandem mass spectrometry, UPLC-MS/MS)
方法 , , UPLC-MS/MS
, 结果 1~100 μg/L , r2 0.990,
, 92%~115%, 3.7 %~6.6%;
1 μg/kg结论 , A
关键词: A; -; ;
Determination of bisphenol A residues in milk by ultra performance liquid
chromatography-tandem mass spectrometry
*
ZHANG Jian-Ying, YANG Xiu-Bin, LUO Yao, JIN Xiao-Lei, YUE Zhen-Feng , Chen Bo
(Shenzhen Key Laboratory of Detection Technology R D on Food Safety, Food Inspection and Quarantine Center,
Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518045, China)
ABSTRACT: Objective To establish an ultra performance liquid chromatography-tandem mass spectrome-
try method for the determination of bisphenol A (BPA) in milk. Methods The residues of bisphenol in the test
samples were extracted with acetonitrile. After being cleaned up with mixed anion exchange solid-phase ex-
traction column, the residues were detected by ultra performance liquid chromatography-tandem mass spe
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