顶空固相微萃取-气相-质谱分析灰树花挥发成分 analysis of volatile components in grifola frondosa by headspace solid phase microextraction-gcms.pdfVIP
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顶空固相微萃取-气相-质谱分析灰树花挥发成分 analysis of volatile components in grifola frondosa by headspace solid phase microextraction-gcms
2013 年 5 月 食品研究与开发
第 34 卷第 10 期 Food Research And Development 分离提取
28
DOI :10.3969/j.issn.1005-6521.2013.010.008
顶空固相微萃取-气相-质谱分析
灰树花挥发成分
李 * ,
晔,王晓杰 金丽华
(北京电子科技职业学院,北京100029)
摘 要 :顶空固相微萃取-气相色谱-质谱法(HS-SPME-GC-MS )分析灰树花挥发性成分。前处理采用干法,顶空固相
微萃取提取后,用气相色谱-质谱联用技术检测灰树花挥发性化学成分。结果表明,共鉴定了 56 种成分,占总成分含
量的 97.9 % ,主要为酯类(51.12 % )、烷烃类(26.97 % )、醛类(7.33 % )和萜烯类(4.90 % )。无溶剂的顶空固相微萃取-
气相色谱-质谱联用技术可以作为灰树花挥发性成分分析的有效方法。
关键词 :灰树花;顶空固相微萃取;气相色谱-质谱;挥发性成分
Analysis of Volatile Components in Grifola frondosa by Headspace Solid Phase Microextraction -GC/MS
*
LI Ye , WANG Xiao-jie ,JIN Li-hua
( , , )
Beijing Polytechnic Beijing 100029 China
Abstract :The headspace solid phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-
MS ) was used to analyse the volatile components in Grifola frondosa. The volatile components in Grifola
frondosa were extracted by HS-SPME with dry pretreatment. Then detected by GC-MS. The GC-MS analysis
results showed that 56 compositions were identified and accounted for 97.9 % of the total peak areas. The major
volatile components included esters (51.12 % ), alkanes (26.97 % ), aldehyde (7.33 % )and terpene (4.90 % ).
HS-SPME-GC-MS strategy would be a useful and feasible method for the analysis of volatile components in
Grifola frondosa.
; ( );
Key words : Grifola frondosa head space-solid phase microextraction HS-SPME gas chromatography-mass
spectrometry ( C-MS )
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