A Study on the deposition of pyrolytic carbons from hydrocarbons英文文献.pdfVIP

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A Study on the deposition of pyrolytic carbons from hydrocarbons英文文献.pdf

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Cnrbon Vol. 22. No. 6. pp. 563-570. 1984 ooO8-6223184 $3.oOC 00 Printed I” the U.S A Pergamon Pres* Ltd A STUDY ON THE DEPOSITION OF PYROLYTIC CARBONS FROM HYDROCARBONS J. H. JE and JAI YOUNG LEE Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, P.O. Box 150 Cheongryang, Seoul, Korea (Received 11 February 1983 and in revised form 15 December 1983) Abstract-A new method for forming isotropic, laminar, and columnar pyrolytic carbons is proposed. For this, a low RPM (below 2.4rpm) tumbling bed has been used to deposit pyrolytic carbons from hydrocarbon gases. All deposits were made on graphite substrates from propane and methane at a constant temperature of 12OO“C.The microstructures of the pyrolytic carbons deposited were dependent on the flow pattern of the reactant gas, the rpm of the reactor, the hydrocarbon concentration, the nature of the hydrocarbon, and the geometry of the bed. Isotropic pyrolytic carbon is formed under deposition conditions where homogeneous nucleation occurs in the gas phase and at the gas flow conditions where the gas-borne droplets can collide on the substrate. Laminar carbon is formed under deposition condition