宽带co2激光制备batio3陶瓷的分析-analysis of batio o3 ceramics prepared by broadband co2 laser.docxVIP

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宽带co2激光制备batio3陶瓷的分析-analysis of batio o3 ceramics prepared by broadband co2 laser.docx

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宽带co2激光制备batio3陶瓷的分析-analysis of batio o3 ceramics prepared by broadband co2 laser

Study on Synthesis of BaTiO3 Ceramica by Wide-Band Laser of CO2AbstractWith the development of electronic products,Barium-titanate functional ceramics of Preparation Method and functional application by some reseacher in many contries. However, the research of barium titanate was began only in recent years in our country and there is a lot of work to do.In the paper the advantages and disadvantages for preparation and performance of Barium-titanate functional ceramics, synthesis of Barium-titanate functional ceramics by wide-band laser sintering. And the basic theory is the solid phase sintering. Bariumtitanate ceramics is characterized by means of Laser Particle Sizer 、XRD、OM、SEM、TG-DSC and Static-of-spring. In general, the main work is as follows:Firstly, the elements powers of BaCO3 and TiO2 with different ball-milling time. Analysis of the milling time on powder properties by means of Laser Particle Sizer and SEM. The best ball-milling time of 16h was fixed by compared the different ball-milling time on powder properties .Secondly ,The elements powers of BaCO3 and TiO2 by the different Parameters of Laser Sintering. And the basic the best ball-milling. The effects of barium-titanate ceramics by the different laser sintering parameters were analysed and changed of structure and performance. The optimum technological parameters for preparingBaTiO3 by wide-band laser sintering is: P=600W、V=60 ㎜/s、f=315 ㎜; The tetragonalbarium titanate ceramics is synthesized by wide-band laser sintering , and its content is up to 91.5% of total, the curie temperature is promoted from 120℃ to 125.9℃,and the density :ρ＝5.5g/cm3.Finally, two kinds of elements were doped by laser sintering. A research was made on influence of Ca2+ or Y3+ contents on the microstructures and mechanical properties of the investigated. Doping different amount of barium-titanate ceramics its structure remains unchanged; when Ca2 ＋ is doped into ceramics, the growth of grain size is restrained, tem