la0.7ba0.3mno3薄膜的应变和气氛退火效应研究-study on strain and atmosphere annealing effect of la 0.7 ba 0.3 mno 3 thin films.docx

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2018-05-27 发布于上海
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la0.7ba0.3mno3薄膜的应变和气氛退火效应研究-study on strain and atmosphere annealing effect of la 0.7 ba 0.3 mno 3 thin films.docx

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la0.7ba0.3mno3薄膜的应变和气氛退火效应研究-study on strain and atmosphere annealing effect of la 0.7 ba 0.3 mno 3 thin films

effectofLBMOfilmandmadeafurtherresearchontheannealingmechanisminthishighlystrainedLBMOfilm.Furthermore,aphaseseparationtendencywasobservedinthinnerLBMO/LAOfilmwhichcouldbeconfirmedundertheassistanceofmicrofabricationtechniquesandthereasonwasanalyzed.Therearefivechaptersinthisthesis,whichcanbepresentedasfollows:Inchapterone,wefirstpresentabriefreviewofthehistoryofCMRmanganite.Next,weintroducesomephysicalpropertiessuchascrystalstructure、J-Tdistortion、electronicstructure、phasediagram,etc.Then,wemakeadetaileddiscussionaboutthepropertiesofmanganitefilms,indicatingthatstraineffectsandoxygencontentshaveacrucialinfluenceonthepropertiesandstructureofmanganitethinfilms.Atlast,wepresentseveralmainmodelswhichareusuallyusedtoexplainthephenomenaemergedinmanganitethinfilms.Inchaptertwo,wefirstintroducesomemethodsaboutfilmpreparationandcharacterization.ThentheseLBMOfilmspreparedbyDCmagnetronsputteringtechniquearecharacterized.Atlast,thestraineffectsarediscussedindetailsandwefindthatthemetal-insulatortransitiontemperatureTPandCurietemperatureTCdecreasewiththereductionoffilmthicknessforoxygenannealedLBMO/LAOfilmsunderahighertemperature,indicatingthatacompressivestrainsuppressesferromagnetismandreducesferromagnetic(FM)CurietemperatureTCinthefilmswhichcanbeinterpretedbytwo-orbitalmodel.Inchapterthere,adetaileddiscussionofthemechanismofannealingonLBMO/LAOthinfilmsismadefirstly.Wefindthattheoxygenatomsinab-planecantransfertoc-axisbyannealingandtheoxygendiffusionofoxygenambienceplaysaminorrole.Arelationshipbetweenthestrainandoxygencontentisobserved,whichcanberepresentedthatalargerin-planecompressivestrainwillcapturemoreoxygeninthisplane.Next,theevolutionofoxygendistributioninLBMOfilmsafteranannealingtreatmentisstudied.Oxygentransferratefromabplanetoc-axisbecomesslowunderanintermediatetemperatureannealingtreatment.Atlast,aphaseseparationtendencyisobservedinthethinnerLBMO/filmsannealedunderanintermediatetemperature,whichcanattributedtocooperativeinteractionofstrainandoxygendistribution.Inch