pztpnnpzn四元系压电陶瓷的低温烧结与性能研究-study on low temperature sintering and properties of pzpnnpzn quaternary piezoelectric ceramics.docxVIP

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pztpnnpzn四元系压电陶瓷的低温烧结与性能研究-study on low temperature sintering and properties of pzpnnpzn quaternary piezoelectric ceramics.docx

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pztpnnpzn四元系压电陶瓷的低温烧结与性能研究-study on low temperature sintering and properties of pzpnnpzn quaternary piezoelectric ceramics

Then, in order to getting specimen which have excellent electrical properties in a low sintering temperature, a amount of CuO was added into PZT-PNN-PZN quaternary piezoelectric ceramics. The experimental results sho w that the add of CuO did not change the main crystal structure, and could clearly improve density. When1mol% CuO was added into specimen, the piezoelectric constant d33, relative33dielectric constant εT /ε0, dielectric loss tanδ of specimen which was sintered at 950°C33for 4h are as follows: d33=411pc/N, εT /ε0=2449, tanδ=1.86%. The method of addedCuO can lower the sintering temperature of PZT-PNN-PZN quaternary piezoelectric ceramics, at the same time havebetter electrical properties.33Finally, Low-temperature sintering of (a-x)Pb(Zr0.48Ti0.52)O3-bPb(Ni1/3Nb2/3) O3-c Pb (Zn1/3 Nb2/3)O3-xPb(Fe2/3W1/3)O3 (a+b+c+x=1, 0.06≤x≤0.10) ceramics were prepared through two-step synthesis process using perovskites-structured ferroelectric materials Pb(Fe2/3W1/3)O3 (PFW) as a sintering aid. The effects of PFW content on the the densification, microstructure, phase structure, dielectric and piezoelectric properties of the ceramics were investigated. The sintering temperature was reduced from 1180 °C (without PFW addition) to 940°C when the material was PFW-doped. PFW-doping increased the sintered density and the average grain size of PFW-PNN-PZN-PZT ceramics. The ceramics sintered at 940 °C for 4h with x=0.08 exhibited favorable properties, which were listed as follows: d33=496pC/N, εT/ε0=3119, tanδ=2.1% and Tc=242°C. These values indicated that the newly developedcomposition might be suitable for multilayer piezoelectric devices application.KEY WORDS: Low-temperature sintering, piezoelectric ceramics, PZT-PNN-PZN， liquid phase目录第一章绪论.........................................................11.1 研究背景及意义 ................................................11.2 低温烧结技术 ..................................................11.2.1 改变配方 ...................