玉米黄色素的超临界co,2萃取及其性质和应用的分析-supercritical co, 2 extraction of zeaxanthin pigment and analysis of its properties and application.docxVIP

摘要- ot玉米黄色素是一种利用价值较高的天然营养色素。我国对玉米黄色素的研究开发 较少，而且一般用有机溶剂法提取，获得的色素产品质量差。本课题针对这一问题，采飞、用超临界 CO2 萃取技术从玉米淀粉加工的副产品一玉米蛋臼粉中萃取玉米黄色素，研究 超临界 C?2萃取和分离过程的试验参数，并对玉米黄色素分析鉴定、性质和应用进行研 究.1.研究超临界 CO2 萃取和分离过程的试验参数，结果表明:采用三因素二次旋转试验设计确定超临界 C{}Z萃取玉米黄色素的最佳工艺条件为:温度 (η38.S.C 、压力(p)36lVfPa、时间(t)lllmi陀利用正交试验 C L9 (t)) 设计得到高质量的色素产品的较优 分离条件为:分离釜 I 压力 9MPa ，分离釜I 温度 4S.C ，分离釜II温度 50-C。2. 脱色玉米蛋白粉在蛋糕、茶肠和冰漠淋中的应用研究结果表明，蛋糕中添加锐 的玉米蛋白粉，冰滨淋中添加 1%的玉米蛋白粉应用效果良好，然而在茶肠中的应用效果较差。3.对两种方法提取的玉米黄色素产品感官指标和理化指标的测定结果说明了超临 界 C02 萃取法优于有机溶剂萃取法。4. 对玉米黄色素成品进行分析鉴定，结果表明其中色素成分为类胡萝卡素，玉米 油成分含有棕榈酸、硬脂酸、油酸、亚油酸等脂肪酸，它们对色素有保护作用 。对色素稳定性影响较大，5. 玉米黄色素稳定性的研究结果表明:光、热、 Fe3和 AI Jφ氧化剂和其它金属离子影响很小 ，糖类物质、酸不影响色素的稳定，碱、还原剂 NCl2S03，、Vc 、油脂抗氧化剂均对色素有保护作用 。6. 玉米黄色素在食品中应用的研究结果表明:添加色素的人造奶油、硬糖色泽鲜艳、感官良好，将其保存三个月，自然光 下色素的吸光度值下降较少，说明玉米黄色素性质』较稳定，完全可以应用到食机)/---?关键询:玉米黄色素超临界 C02 萃取性质应用\/\Study 00 Extraction of Maizeyellow Pigment with Supercritical CO2 aod Its Properties and ApplicationABSTRACTMaizeyellow pigment is a natural nutrient p韧lent wìth high vωe of uti1ization. Studieson it are few in our country. Maizeyellow pigment is commonly extracted by using organic?solvent but the quality of the acquired pigment is bad. This subject ís to extract maizeyellowpigment from maize protein powder by using supercritical C?2 which is a byproduc1 of mruzestarch processing. It studies the experimental p缸缸neters in the process of supercritical CO2fextraction of maizeyellow pigment and its identification and prope均 and application.a‘Study on the experimental par缸neters of supercrit比al C02 extraction showed that a mathematical model of the second power of three factors was set up in order to identify 由e optimal technical condition. It was that temperat山它 is 38.8.C ，pressure is 36Mpa and tíme is 111rninutes . High quality maizeyellow pigment was obtained by using the orthogonal( 4 ( 34 )) test and the better separation condition was that the pressure of separation vessel 1 is9Mpa and 由e temperature is 45 0Cand the temperature of sepration vessel lI is 50.C