Discovery Based Learning Using NMR Spectroscopy利用核磁共振光谱的学习为基的发现.pptVIP

Transition to an Investigative Laboratory Program in Chemistry at Birmingham-Southern College David J. A. Schedler and Laura K. Stultz Introduction National Science Foundation Grant Investigative Laboratories Development of Laboratory Projects Examples Project Goals Student Goals Improve - Problem solving and collaborative skills - Ability to apply experimental techniques to solve a chemical problem. - Ability to communicate results (written and oral) Investigative Laboratories Students discover results instead of verifying them Experimental protocols are largely student designed Work is done in collaborative groups Interpretation of results through data analysis Group discussion First Semester Focuses on Techniques and Instrumentation Distillation Crystallization Melting point TLC GC NMR Second Semester Focuses on Application NMR FT-IR Molecular modeling Stereochemistry and Coupling Constants Projects should have clearly stated: Objective Outcome Introduction Theory for the instrumentation to be used background into the chemistry involved Experimental Procedure Diels-Alder Reaction prediction of reaction product carry out reaction using previously learned lab techniques Electron Transfer Self Exchange Rates Kinetic NMR experiment Factors that affect the electron transfer rates Acknowledgements National Science Foundation (Award DUE-0126478) Dr. Regina Stanton Mr. Patrick McTamney Ms. Karen Johnson Mr. Nathan Boyd Birmingham-Southern College /chemistrylabs.htm * * Curricular Goals Improved laboratory experience Better synergy between lecture and laboratory Connections between chemistry courses Project Plan Gradualism Model – stepwise presentation of new material with specific goals Instrumental techniques as common thread - Molecular Modeling - FTNMR (1H and 13C) Project based Laboratories – Reinforces concepts and skills Student involvement in laboratory design 1.34 kcal/mol 2.39 kcal/mol 12 180 HaxCCHax 4 12 180 HaxCCHax 3 2.5 60 HaxC