纳米cupmma微发泡复合材料的制备及其力学性能研究-preparation and mechanical properties of nano cup mma microcellular foam composites.docxVIP
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纳米cupmma微发泡复合材料的制备及其力学性能研究-preparation and mechanical properties of nano cup mma microcellular foam composites
高的微发泡材料在静态加载实验中有明显的屈服平台,在动态加载条件下有较强的应力波弥散效应,均具有良好的吸能作用,具有优异的抗爆性能。关键词:原位还原技术,异相成核剂,超临界二氧化碳发泡技术,纳米Cu/PMMA微发泡复合材料,力学性能IIAbstractNanoCopper/PMMAmicrocellularfoamshavethemultifunctionoflightweightwithcompressivecapacity,explosion-proofperformanceandhighstrengthduetoexistingalargeamountofmicrocellular.Sotheyhavewidelyusedinthefieldsofpackaging,communicationandtransportation,automobileindustryandnationaldefense.Inthisarticle,coppernanoparticleswereembedinPMMAastheheterogeneousnucleatingagentbyinsitureductionmethod.TheCopper/PMMAmicrocellularfoamsweresynthesizedthroughsupercriticalcarbondioxide(ScCO2)foamingtechnology.Inthisresearch,wefocusoninvestigatingtheinfluenceoffoamingconditionsonmicrocellularsstructureandmassdensity.Themechanicalpropertiesatquasi-staticandhighstrainratewerealsostudied.Firstly,monodispersedcopper/PMMAcolloidswereobtainedbyinsitureductionmethodwhichcopperchloridedihydrate(CuCl2?2H2O)usedastheprecursorofcoppernanoparticleswhileN,N-dimethylformamideactedasreducingagentintheabsenceofanystabilizers.ThecoppernanoparticlescontentwaseasycontrolledbythequantityofcopperchloridedihydrateinDMF.Theeffectofcoppernanoparticlecontentondispersityofcolloidswasinvestigated.Whenthecoppercontentlessthan10wt.%,thenearlysphericalcoppernanoparticleshavehighdispersitywithanarrowsizedistribution.Whilethecontentexceed10wt.%,thenearlysphericalcoppernanoparticleswouldbeagglomeration.So,thecoppercontentofcopper/PMMAnanocompositescanbedeterminedtosynthesisCopper/PMMAmicrocellularfoamswithhighfoamingefficiency.Secondly,thecopper/PMMAnanocompositesweresynthesizedthroughanti-solventprecipitationmethodandhotpressingmoldingtechnology.TheCopper/PMMAmicrocellularfoamsweresynthesizedthroughsupercriticalcarbondioxidefoamingtechnology.Lewisacid-basetheory,whichisthetheoreticalbasisoftheinteractionofScCO2andPMMAwasdiscussed.TheadsorbingcapacityofCO2inPMMAwasmeasuredbygravimetricanalysis.Thesaturationtimeoffoamingprocesswas8hoursbasedontheadsorbingcapacityofCO2inPMMA.Theinfluenceofsaturationt
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