γ-TiAl基合金的脉冲电流烧结与成形性能-材料加工工程专业论文.docxVIP

哈尔 哈尔滨工业大学硕士学位论文 哈尔 哈尔滨工业大学硕士学位论文 - - PAGE IV - - - III - Abstract γ-TiAl based alloys are promising candidates for elevated temperature structural materials due to their superior characteristics, such as low density, high young’s modulus, excellent strength and oxidation resistance at elevated temperature. However, they suffer from room temperature brittleness and poor workability, hindering their applications. The grain size has a very important effect on the properties of material. However,it is difficult to prepare TiAl alloy with fine and homogeneous microstructure by traditional casting and mechanical working processes. Pulse Current Auxiliary Sintering(PCAS), because of its quick heating rate, short sintering time, controllable microstructure, high material density, is videly used to produce TiAl alloys with refined microstructure. In this paper, TiAl based alloys from the prealloyed powder of were prepared by pulse current auxiliary sintering. In the synthesis process, influences of different parameters, including heating-up rate, sintering temperature and duration time, on obtained microstructures in sintered products were studied. Effect of microstructure on properties at elevated temperature was tested. High tensil properties were obtained at relatively low temperature. Based on the tensil properties, superplastic extrusion of blade was conducted. Pulse Current Auxiliary Sintering: When powders were synthesized in the oven at 1250℃ for 5min with heating rates of 4.5, 3.8, 3, 2.5, 2℃ , near gamma, duplex, nearly lamellar, fine fully lamellar and coarse fully lamellar microstructures were obtained, correspondingly. Fine grain size was abtained. The grain size of near γ microstructure has reached 4 μm。 Tensile testing at elevated temperature: Tensile tests of different microstructure were conducted in temperature range of 950℃~1000℃. The results showed that one with equi-axed fine grains possessed more superior elevated temperature tensile properties. Wh