表面机械研磨处理az31镁合金显微组织和力学性能研究-材料加工工程专业论文.docxVIP

AB ABSTRACT I III ABSTRACT In recent years, gradient nano structure materials have attracted much attention due to these special microstructure and excellent properties. Surface mechanical attrition treatment (SMAT), as the most effective surface nanocrystallization way to obtain the gradient nano structure, has been successfully applied to copper, nickel, stainless steels and other metal materials, and has made significantly improvement in their mechanical properties. However, there are few reports on the mechanical properties of magnesium (Mg) alloy with gradient nano structures. Therfore, in the present work, SMAT has been carried out on the AZ31 Mg alloys prepared by equal channel angular pressing (ECAP) and commercial rolling, respectively. By means of optical microscopy (OM), X- ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), microhardness test and mniaxial tensile test, the microstructure and mechanical properties of the AZ31 Mg alloys with SMAT are investigated. The effect of SMAT on the microstructure and mechanical properties of the two types of AZ31 Mg alloys has been discussed and analyzed. Finally, the dynamic tensile deformation behavior and fracture behavior of the AZ31 magnesium alloy with gradient structure for different grain sizes have been studied by using SEM in situ tensile test. The main conclusions are as follows: After SMAT, a gradient nano structure is formed in the surface of the ECAPed AZ31 Mg alloy along the thickness direction. The surface layer of the alloy subjected to SMAT for 10 min consists of nanosized grains with an average grain size of 27.4 nm and random crystallographic orientations. The thickness of the nanocrytalline surface layer is about 50μm. Then an ultra-fined grain layer appears to the depth about 80 μm to 90 μm. Below about 90 μm depth are typical as-received structures, but with a certain volume fraction of twins induced by SMAT. After SMAT for a long time, the volum