层状液晶体系中TiO2纳米材料的制备及催化性能研究化学工程专业论文.docxVIP

morphology and size of the products. The formation mechanisms of different shape samples were discussed. A novel, simple and effective method to prepare TiO2 nanomaterials with controllable size and shape was developed in this work. The structure of lamellar liquid crystal has an important effect on the shape and size of the final products. The structure and performance of nanomaterials can be controlled by adjustment of the composition of the lamellar liquid crystal. It is expected that this method can be used to prepare other nanomaterials with specific performance. KEY WORDS：lamellar liquid crystal, template method, capping agent, TiO2, nanomaterials 目 录 HYPERLINK \l _bookmark0 第一章 文献综述1 HYPERLINK \l _bookmark1 1.1 纳米科技1 HYPERLINK \l _bookmark2 1.2 纳米材料的基本知识1 HYPERLINK \l _bookmark5 1.3 制备方法3 HYPERLINK \l _bookmark6 1.3.1 物理法3 HYPERLINK \l _bookmark8 1.3.2 化学法4 HYPERLINK \l _bookmark10 1.3.3 自组装法5 HYPERLINK \l _bookmark12 1.3.4 模板法5 HYPERLINK \l _bookmark13 1.4 模板法构建纳米材料的研究进展6 HYPERLINK \l _bookmark14 1.4.1 模板的分类6 HYPERLINK \l _bookmark15 1.4.2 模板法构建纳米材料的制备技术6 HYPERLINK \l _bookmark19 1.5 LLC 模板法制备纳米材料的研究进展 10 HYPERLINK \l _bookmark20 1.5.1 LLC 的形成及结构特点 10 HYPERLINK \l _bookmark23 1.5.2 LLC 的研究手段 11 HYPERLINK \l _bookmark28 1.5.3 LLC 模板法合成和组装纳米材料 14 HYPERLINK \l _bookmark36 1.6 选题思路和主要内容19 HYPERLINK \l _bookmark37 1.6.1 选题思路19 HYPERLINK \l _bookmark38 1.6.2 主要内容19 HYPERLINK \l _bookmark39 第二章 实验部分21 HYPERLINK \l _bookmark40 2.1 药品及试剂21 HYPERLINK \l _bookmark42 2.2 设备及仪器22 HYPERLINK \l _bookmark45 2.3 溶液的配置22 HYPERLINK \l _bookmark46 2.3.1 TiOSO4 溶液的配制 22 HYPERLINK \l _bookmark47 2.3.2 NH3·H2O 溶液配制 23 HYPERLINK \l _bookmark48 2.4 溶致液晶和样品的表征23 HYPERLINK \l _bookmark49 2.4.1 溶致液晶的表征23 HYPERLINK \l _bookmark50 2.4.2 TiO2 样品的表征 23 HYPERLINK \l _bookmark51 第三章 TX-100/H2O 层状液晶体系中 TiO2 纳米材料的合成研究 25 HYPERLINK \l _bookmark52 3.1 引言25 HYPERLINK \l _bookmark53 3.2 溶致液晶的配制26 HYPERLINK \l _bookmark54 3.3 纳米材料的制备26 HYP