GMS定量标准曲线操作.docVIP

1.首先打开后处理 1.首先打开后处理Postrun, 准样品的图谱;如下所示: GCMS定Ul:标准曲线操作 IGCMS Postrun Analysis^ 缺捷方式 I Lkb ，进入后在Quantitative里打开标 0j 2.5 TIC A MIC Scan J：x100,000,000) TjGCMS Postrun Analysis (Admin) - [Data Analysis -裹 HSOl QQ】 说[ile Compound Table View Qualitative loots Window Kelp #1 Peak Lotd Method 華3 Qutnti ttivParameters xk Ftk Integration 蟬 Calculation 崑 Report Guide -!□! X| -Iff! x| ? [Scan 1 ? IGroup Max Intensity: 49,922,792 Time 19 233 Scan# 2.069 Inten. 69,399,725 Oven Temp260 00 前0714t?t001 0]CI TEST01 团CI TEST02 ?EI TEST001 ?EI TEST002 El TEST003 NCITEST01 NCITEST02 sampl te$t01 sampl test02 sampl testO3 sampl te$tO4 sampl t?tO5 毐鼠强01 奉死蜱-noi AnalyzAdmin Analyz2005-7 Acq. ttScan Sampl eUnknov Level 1 Sample Descri 5.0 10.0 12.5 17.5 20.0 2.0 20 (x1,000,000) 3 0- : 10」 :rc 2.5 Max Intensity: 49,922,792 Time 16.574 Scan# 1.750 Inten. 2,090,906 Oven Temp235.74 7.5 10.0 12.5 15.0 17.5 20.0 10.0^ 7.5」 5.0； 2.5」 0.0」一0.0000 7.5- 5.0- ▼ 一盞 2.5- 0.0- 0.0017 C00100 gBttch Ttbl*|[^Ctlibr亀t... Data Ant... I /人Ready /人 2.然后对目标物色谱图进行扣除背景［-］，再在EDIT下输入目标物名称，M/Z，保留时间和浓 度.如下图所示： 餐JgCMS Postrun Analysis (Admin) - [Data Analysis -塞鼠强01.QGD] File Compound Table Wew Qualitative Quantitative Layout Tools Wfindow Help 这|B| ^lBt| fTBjQ Jj| d 么|3| fol lidilfid 糾滿|刮㈣边I ? |』| 汕秘IlllP di Data Explorer 2d Quantitative Project in TIC MIC Scan \Proj*ctl File Name 70 (100.000.000) Max Intensity: 49,92 2792 ? f气 Time 18.311 Scan# 1,958 Inten. I 62,461,068 Oven Temp2! 53.H Peak Scan Group 7.5 10.0 12.5 15.0 17.5 20.0 LoadMethod Quant i ativeFtrameters ik Peak Int?(rtion 囲匿 Ctlculti(*n 崑 Report Guide ]0714test001 )CI TEST01 jd TEST02 )EI TEST001 )EI TEST002 |?EI TEST003 )NCI TESTO1 ]NCI TEST02 jsampl testOl 」《mpl te$t02 | jsampl test03 ^sarr^l test04 Jsampl test05 ffiwaoi |O 表死S$-EIO1 I Inten. 1.0- 0.0- 11.25 11.50 2.0 20 JZ AntlyzAdmin Analy22005-7 Acq. UScan SampleUnknow Level 1 Stmplt?死碑 Sample Descri tt 1 m/z Abs. Inten. 2 [0 92 132 58,iogH9 281 381 Ret.Time: (11.725]- [11.808] Scantt: (11