水溶性环氧树脂的锆钛酸铅压电陶瓷凝胶注模成型-NSFC.PDFVIP

24 3 2014 3 Volume 24 Number 3 The Chinese Journal of Nonferrous Metals March 2014 1004-0609(2014)03-0773-06 ( 410083) (NH PAA) 4 ()0.6% () 57.5% 55% 34.1 77.8 MPa TN304 A Gelcasting of lead zirconate titanate prepared by water-soluble epoxy resin ZHAO Yang, XIE Rui, ZHANG Yan, ZHOU Ke-chao, ZHANG Dou (State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China) Abstract: The lead zirconate titanate slurry was prepared using polyacrylic acid amine (NH PAA) and Hydantion epoxy 4 resin as dispersant and gelling agent, respectively. The influences of the dispersant content and the solid loading on the rheological properties and physical properties of the green and sintered bodies were investigated. The results show that the viscosity of the slurry is the lowest when the dispersant content is 0.6% (mass fraction). The slurry maintains good fluidity as the solid loading reaches as high as 57.5% (volume fraction). The highest strengths of green and sintered bodies are 34.1 and 77.8 MPa, respectively, as the solid loading of the slurry is 55%. Compared with the die pressing, the gelcast sample exhibits better physical and piezoelectric properties. Key words: gelcasting; lead zirconate titanate; soluble epoxy resin; rheological property [1−2] 20 90 OMATETE [7−9] [3] / [4] [5] [6]