废水中的丙溴磷气相色谱分析-环境监测管理与技术.PDFVIP

14 4 2002 8 监测技术 1 2 2 2 2 史毓华, 朱仁康, 夏豪刚, 王逸虹 , 侯定远 ( 1. 苏州工业园区环境监测中心站, 江苏 苏州 215021; 2. 苏州市环境科学研究所, 江苏 苏州 215004) : , ( N PD) ( ECD) , , 0 . 002 mg/ L( 2 pg, NP D) 0. 000 8 mg/ L ( 0 . 8 pg , ECD) , , , : ; ; : O6577 1 : B : 1006- 2009( 2002) 04- 0033- 02 Analyti cal Method for Prof enofos in Wastewater by GC 1 2 2 2 2 SH Yuhua , ZH U Renkang , X A Haogang , WANG Yihong , HOU Dingyuan ( 1. Suz hou I ndustrial Park s Environmental M onitoring Station, Suz hou, Jiangsu 215021, China ; 2. Suzhou Environmental Sciences I nstitute, Suz hou, Jiangsu 2 15004, China) Abstract:Analytical method for pr ofenofos in wastewater by G C was researched. Profenofos was separated in lar ge caliber cap illary column, and detected w ith N PD and ECD. T he detection limit was 0 . 002 mg/ L( the lowest absolute detection quantity can r eached 2 pg , N PD) and 0 . 000 8 mg/ L ( t he lowest absolute detectio n quantity can r eached 0. 8 pg, ECD) . n this method, the use of twocolumn and twodetectors can eliminate the disturbance of other materials and guarantee the analytical result s reliability. Key words: Profenofos; G S; Wastewater ( Prof enofos) , , , [ 1] , 100 m L , g/ L , , , 01 mg/ L , 13 色谱条件 , 131 HP- 1 ; 200 ∀ ( 1 min) , 20 ∀ / min , , , 270 ∀ ( 1m in ) ; 2 20 ∀ ; , 2 2 0 ∀ ; ( ) 17 6 mL / min ; , HP -