1扫描电镜试样制备.docVIP

PAGE \* MERGEFORMAT8 扫描电镜在木基材料阻燃研究中的应用 基金项目：浙江省重点科技创新团队项目（2012R10023-13），木竹产业技术创新战略联盟科研计划（TIAWBI 201203） 吴再兴，陈玉和，包永洁，邹怡佳 (国家林业局竹子研究开发中心 杭州 310012) 摘要：简要介绍了木基阻燃材料试样的制备方法，以及加速电压、放大倍数等观测条件及其选择方法，从形貌观察、成分分析和微观测量三个方面总结了扫描电镜在木基材料阻燃效果和阻燃机理研究中的应用及存在的不足，指出扫描电镜观测结果的量化表征对于提高不同研究结果的可比性以及阻燃机理的阐明都是是一个有意义的发展方向。 关键词：形貌；成分分析；微观测量；定量表征 Applications of SEM in Research of Flame-Retardant Treatment of Wood-based Materials WU Zai-xing, CHEN Yu-he, BAO Yong-jie, ZOU Yi-jia (China National Bamboo Research Center, Hangzhou 310012) Abstract Preparation of samples and observing conditions for SEM(Scanning Electron Microscope）were introduced briefly, and applications of SEM in research of flame-retardant effect and mechanism of wood-based materials in the aspects of morphology observation, element distribution analysis and micro-measurement and its shortages were summarized. At last, it’s a meaningful developing trend to adopt quantitative characterization instead of qualitative photo, for compare different studies and expound flame retardant mechanism much more reliable. Keywords morphology; element analysis; micro-measurement; quantitative characterization 木基材料的主体是木材及其加工剩余物，而木材是由碳、氢、氧等元素组成的有机化合物,受热会分解,具有可燃性，据统计,21%火灾由木材等纤维材料引起,住宅火灾70%是因木材和木质材料缺乏耐火性而引起 ADDIN EN.CITE EndNoteCiteAuthor廖红霞/AuthorYear2008/YearRecNum14610/RecNumDisplayTextstyle face=superscript[1]/style/DisplayTextrecordrec-number14610/rec-numberforeign-keyskey app=EN db-id=frd2xp2pu9vvfxedwfqxrad6p2eppfxsfvp214610/key/foreign-keysref-type name=Journal Article17/ref-typecontributorsauthorsauthor廖红霞/authorauthor刘磊 /authorauthor谢桂军/authorauthor云虹 /authorauthor郭琼/author/authors/contributorsauth-address华南农业大学林学院;广东省林业科学研究院;/auth-addresstitlestitleSBB防护剂处理木材湿胀性、力学性能及阻燃性能等效果的研究/titlesecondary-title广东林业科技/secondary-title/titlesperiodicalfull-title广东林业科技/full-title/periodicalpages22-25/pagesnumber01/numberkeywordskeywordSBB防护剂/keywordkeyword湿胀性/keywordkeyword力学性能/keywordkeyword阻燃性能/keyword/keywordsdatesyear2008/year/datesisbn1006-44