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- 2019-06-05 发布于广东
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Preparation of PMPS Chelating Fibers A glass fiber substrate was dip-coated with a MPS-10% (or MPS-20%) solution for 1 min, and placed on a fine mesh screen. The coated glass fibers were dried in a hood at room temperature for 30 min. PMPS 螯合纤维的制备: 用MPS - 10 %(或MPS - 20 % )浸泡玻璃纤维衬底1分钟,然后放在一个优良的筛网上。该涂覆的玻璃纤维,在室温下在通风橱中干燥30分钟。 The dried fibers were cured at 80 °C for 12 h and then at 120 °C for 48 h in a vacuum oven. The cured fibers were allowed to cool toroomtemperature slowly and weighed immediately. 翻译: 在80℃下固化12小时,干燥后的纤维置于120℃下在真空烘箱中48小时。固化的纤维被允许慢慢冷却到室温并马上称重 The final thiol-functionalized chelating fibers prepared from MPS-10% and MPS-20% coating solutions are designated as PMPS-10% and PMPS-20%, respectively. 翻译: 最后带硫醇官能团的螯合纤维准备置于MPS -10 %和MPS -20 %涂层溶液中,分别被合成为10%聚甲基苯基硅氧烷, 和 20 %聚甲基苯基硅氧烷。 Weight gains for the PMPS-10% and PMPS-20% fibers after coating were 50% and 85%, respectively. 翻译: PMPS-10%和PMPS-20%重量分别增加了50%和85% We will synthetise AEAPS ,Thiol-Functionalized Polymercaptopropylsilsesquioxane (PMPS) Chelating Fibers, PAEAPS like the way before.For time reason,I am not likely to talk about it . Synthesis of PMPS fibers Results and Discussion Thiol functional groups have been recognized to be efficient chelating ligands for mercury and other heavy metals such as lead and silver. 结果与讨论 巯基官能团已确认为汞,铅,银等重金属离子有效的螯合配位体。 Here, we incorporate the thiol groups into the side chains of cross-linked polysilsesquioxane coated glass fibers in order to efficiently remove mercury from contaminated aqueous solutions. 翻译: 在这里,我们把巯基结合到涂覆在玻璃纤维上的聚倍半硅氧烷的侧基上,以有效地除去被汞污染的水溶液。 Conclusions: Two new classes of chelating fibers, polymercaptopropylsilsesquioxane (PMPS) and copper(II) ferrocyanide complexed poly[1-(2-aminoethyl)-3-aminopropyl]silsesquioxane (Cu-FC-PAEAPS) fibers, have been synthesized for the selective removal of trace amounts of mercury and cesium ions, respectively, from water, in the presence of competing metal ions. 结论: 我们已经合成了两种新型的螯合物纤维。PMPS和亚铁络合铜(II)聚[1 - ( 2 -
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