新酪啡肽Fmoc固相合成及其活性的检测.pdf

● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 2O ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 20 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 20 ● ， ■ ● ● ● ● ● ● ● ● ● ● ● ● ● 20 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 21 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ■ 21 ● r■ ● ● ● ● ● ● ● ● ● ■ ● ● ● 21 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 22 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 22 ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● ● 22 ● ● ● ● ● ● ● ● ■ ● ● ● ● ■ ● ● 22 2．6 酪啡肽的抗疲劳作用……………………………………………………………．．22 2．6．1 实验材料与仪器……………………………………………………………．．22 2．6．2 实验方法……………………………………………………………………．．23 第三章结果………………………………………………………………………………………．24 3．1 酪啡肽固相合成条件的确定………………………………………………………24 3．1．1 接肽反应时间的确定…………………………………………………………24 3．1．2 洗涤方法的确定……………………………………………………………．．25