年产5万吨工业级甲醛的工艺设计甲醇的预热器的设计.docxVIP

PAGE 1 PAGE 22 年产5万吨工业级甲醛的工艺设计 —甲醇的预热器的设计 摘 要：甲醛是重要的化工产品。这篇文章主要介绍了甲醛的性质、用途、主要生产方法、市场前景及发展趋势；设计了年产5万吨工业级甲醛的生产工艺；选用铁钼法，以甲醇为原料，经甲醇预热、甲醇的蒸发、换热器、反应釜反应后得甲醛产品。本文主要承担甲醇预热器的设计，根据物料衡算及热量衡算结果，确定了预热器的工艺参数、类型及特征尺寸：公称直径 250mm、公称面积 9m2、管数 20、管长 6m；采用浮头式换热器，管束的排列方式采用正三角形排列，弓形折流挡板。并对换热器进行了流力学和热力学的核算.结果表明所设计的换热器符合要求。 关键词：甲醛；工艺设计；预热器 Process design of industrial formaldehyde Of 50,000 tons per year —the design of Heat Exchanger Lixiaoping (Department of Chemistry and Chemical Engineering, Baoji University of Arts and Sciences, Baoji, Shaanxi,721013) Abstract: Formaldehyde is important chemical products. This article mainly introduced the formaldehyde properties, applications and the main production method, the market prospect and development tendency; The annual 5,000 tons of industrial design formaldehyde production craft; Choose iron molybdenum law to methanol as raw materials, the methanol preheating, methanol evaporation, heat exchangers, reactor reaction to formaldehyde products. This paper mainly undertakes methanol preheater design, according to the material calculation and heat calculation results to determine the preheater parameters, type and feature sizes: nominal diameter 9m2 250mm, nominal area, tube length number 20, 6m; Using FuTou heat exchanger, bundle arrangement the positive triangle is arranged, bow baffle platens. And the flow of heat exchanger accounting of mechanical and thermodynamics. Results showed that the design meets the requirements of heat. Key words: formaldehyde; Process design; preheater  目录 TOC \o 1-3 \h \z \u 1.概述 1 1.1性状及用途[1] 1 1.2甲醛的生产工艺 1 1.2.1银催化法生产甲醛 2 1.2.2 ?铁钼法生产甲醛 4 1.2.3其他方法 5 1.3国内外生产概况 7 1.4市场需求及发展前景 8 2. 原料、辅助原料、产品的主要技术规格 10 2.1银法和铁钼法生产甲醛的技术经济指标 10 2.2 原料规格 11 表1 原辅料规格及消耗配比[5] 11 2.3 产品质量标准 11 3. 工艺介绍 12 4. 换热器设计方案的确定 13 5.换热器的工艺计算 13 5.1 确定物性数据 13 5.2 计算冷却剂用量 14 5.3 计算传热面积 14 6. 工艺尺寸计算 15 6.1 管径 15 6.2 管子数 15 6.3 传热管排列 15 6.4 壳体内径 15 6.5 折流板 16