_石墨炉加热法测定土壤中有机质的含量.pdfVIP

第28卷 第3期 湖 南 城 市 学 院 学 报 （自然科学版） Vol.28 No.3 20 19年 5月 Journal of Hunan City University （N atural Science ） May 20 19 石墨炉加热法测定土壤中有机质的含量 尹志芳，曾偲祥 (湖南城市学院 黑茶金花湖南省重点实验室 ，湖南 益阳 413000) 摘 要：土壤有机质含量是评价土壤肥力的一个重要指标，采用重铬酸钾氧化法对土壤有机质含量进行 测定，得到石墨炉加热法测定土壤有机质含量的最佳消解温度为220 ℃，消解时间为10 min﹒石墨炉加热法和 油浴加热法进行对比研究，2种方法相对标准偏差分别为0.86%和1.70%，说明石墨炉加热法精密度优于油浴 加热法﹒在最优条件下测定5种土壤样品中的有机质含量，平行测定5次，最大相对标准偏差为0.91%﹒ 关键词：土壤有机质；重铬酸钾氧化法；石墨炉加热法；油浴加热法 + 中图分类号：S151.9 5 文献标识码：A doi:10.3969/j.issn.1672-7304.2019.03.0016 文章编号：1672–7304(2019)03–0074–05 Determination of Soil Organic Matter Content with Graphite Furnace Heating YIN Zhifang, ZENG Sixiang (Hunan Provincial Key Lab of Dark Tea and Jin-hua, Hunan City University, Yiyang, Hunan 413000, China) Abstract: The soil organic matter content is an important index for evaluating soil fertility. Potassium dichromate oxidation method is used to determine soil organic matter content. The optimum digestion temperature for determining soil organic matter content by graphite furnace heating method is 220 ℃ and the digestion time is 10 minutes. The relative standard deviations of the graphite furnace heating method and oil bath heating method are 0.86% and 1.70% respectively, which shows that the precision of graphite furnace heating method is better than that of oil bath heating method. Under the optimum conditions, the content of organic matter in five soil samples is determined. The maximum relative standard deviation was 0.91% after five parallel experiments. Key words: organic matter content; met