英文改性纳米TiO2交联羟丙基瓜尔豆胶的凝胶化、性能及微观形貌研究.pdf

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ArabianJournalforScienceandEngineering(2022)47:7001–7011

/10.1007/s13369-021-06242-x

RESEARCHARTICLE-CHEMISTRY

StudyonGelation,PropertiesandMicromorphologyofModiﬁed

Nano-TiO2CrosslinkingHydroxypropylGuarGum

FuChen1,2·YuDeng1,2·KunyiHe3·MinaLuo1,2·JieHe1,2

Received:11March2021/Accepted:20September2021/Publishedonline:31October2021

©KingFahdUniversityofPetroleumMinerals2021

Abstract

Inthestudy,ahydroxypropylguargum(HPG)gelwaspreparedusingmodiﬁednano-TiO2particlesasacrosslinking

agent.Firstly,nano-TiO2particleswerepreparedusingthesol–gelmethod.Nano-TiO2particlesweresphericalanddensely

distributed;theeffectiveparticlesizewas29.0nm,andparticlesizedistributionwasuniform.Then,themodiﬁednano-TiO2

particlesweresynthesizedbymodifyingnano-TiO2withpolyhydroxycarboxylate.Themicrostructureofnano-TiO2and

modiﬁednano-TiO2crosslinkedHPGgelwereinvestigated.Thelayereddistributionandcrosslinkednetworkofthemodiﬁed

nano-TiO2gelweredenserthanthatofnano-TiO2crosslinkedHPGgel.Themodiﬁednano-TiO2crosslinkedHPGgelshows

stableviscoelasticityat60°C.Comparedwithnano-TiO2crosslinkedHPGgel,ithasbettertemperatureresistanceandshear

resistance,andcanadapttoformationfracturingat140°C,indicatingthatthisgelmayhavepotentialapplicationinfracturing.

KeywordsModiﬁednano-TiO2particles·Fracturingﬂuid·HPGgel

1Introductionandgalactosebranch[5].Asanimportantadditiveoffrac-

turingﬂuidsystems,theperformanceofcrosslinkingagents

Asdemandforoilgrowsandtechnologycontinuestoevolve,directlyaffectsthetemperatureresistanceoffracturingﬂuid

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