蔬菜中有机磷农药残留量的检测与分析-本科生毕业论文.docVIP

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黑龙江东方学院

本科生毕业论文

蔬菜中有机磷农药残留量的检测与分析

姓名

学号

专业食品科学与工程

班级

指导教师

学部食品与环境工程学部

答辩日期

黑龙江东方学院本科生毕业论文

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蔬菜中有机磷农药残留量的检测与分析

摘要

有机磷农药作为一类高效、广谱的杀虫剂正被广泛地用于农业防害以及家庭、仓储等的杀虫，但大量使用后产生的环境危害也日益严重。农药的急性中毒，特别是果蔬食品污染后引发的群体中毒事件屡有发生。因此建立果蔬有机磷残留检测技术是很有必要的。

本课题采用乙腈浸提，同时对茄果类、瓜类、甘蓝类、白菜类、绿叶类、豆类6类蔬菜共24个品种，采用气相色谱法检测有机磷中高毒农药甲胺磷、氧化乐果、甲拌磷、对硫磷、甲基对硫磷、毒死蜱、敌敌畏、乙酰甲胺磷、三唑磷、杀螟硫磷、水胺硫磷等13种农药残留情况。本次检测蔬菜样品24个，其中检出含有被测农药样品8个，检出率33.3%；被测农药不合格的样品3个，总合格率87.5%。有5种高毒农药被检出，其中毒死蜱的检出率最高，达到25%，氧化乐果的检出率为16.7%，甲胺磷、水胺硫磷、乙酰甲胺磷均为8.3%。

关键词：气相色谱；有机磷农药；蔬菜

Vegetablesintheorganicphosphoruspesticideresiduesinthedetectionandanalysis

Abstract

Theganophosphorusagriculturalchemicalstakeonekindhighlyeffective,GuangPuthepesticidewidelytouseinagriculturalagainstevilaswellasthefamily,thewarehousingandsooninsectdisinfestation,butusesaftermassively,producestheenvironmentharmdaybydayisalsoserious.Agriculturalchemicalsacutepoisoning,afterspeciallyfruitsandvegetablesfoodcontamination,initiatesthecommunitypoisoneventsometimesoccurs.Thereforetheestablishmentfruitsandvegetablesganophosphorusremainstheexaminationtechnologytohavethenecessityverymuch.thistopicusesthemethylcyanidetosoakraises,simultaneouslytotheeggplantfruitclass,themelonclass,theseacabbageclass,thecabbageclass,thegreenleafclass,thelegumes6kindofvegetablesaltogether24varieties,usesinthegasphasechromatographyexaminationganophosphorusthehighpoisonousagriculturalchemicalsmethylaminephosphorus,theoxidizedrogor,thethimet,theparathion,themethylparathion,tokillbypoisonthetick,thephosphateinsecticide,theacetylmethylaminephosphorus,thetriazolephosphorus,tokillthesnoutmothsulfurphosphorus,ShuiAnliuthephosphorusandsoon13kindofpesticideresiduesituation.Thisexamin