【化学工程与工艺专业】【毕业设计+开题报告+文献综述】纺锤形Fe2O3及Fe2O3@Au核壳纳米粒子的制备及表征.doc

（20 届） 毕业设计 纺锤形Fe2O3及Fe2O3@Au核壳纳米粒子的制备及表征 摘 要随着纳米科技的快速发展，可控制备特殊结构的纳米材料已经成为可能由此产生强的SERS效应强迫水解法选取晶体助剂为KH2PO4，浓度为4×10- 4 M100℃下水解FeCl3。 Abstract In recent years, metal and composite nano-materials research in many areas of the great role played by the great interest aroused, the following two main reasons: first because of their nanometer-sized nanoparticles produced by the unique chemical physics, optical , electronic properties, and its practical application in basic research has great value. The second effect of the surface of nano-materials, nano-particles make the surface atoms and the particles with adsorbate contact surface between the maximum, so that the nanoparticles in catalysis has tremendous potential value. With the rapid development of nanotechnology, the special structure of the controllable preparation of nano-materials has become possible. By different physical or chemical methods, controlled synthesis of nanocrystals with different morphologies and study functional characteristics of nanostructures is a very important issue. With special appearance of the nano-materials have novel optical, electrical, magnetic, and chemical properties, especially the adjustable optical properties, such as surface plasmon resonance, the resulting strong SERS effect, have attracted particular attention. The use of forced hydrolysis method, select additives for the crystal KH2PO4, the concentration of 4 × 10 - 4 Mol / L, 100 ℃ hydrolysis of FeCl3 available under the spindle Fe2O3. Fe2O3 @ Au core-shell nanoparticles is the use of hydroxylamine hydrochloride in the Fe2O3 surface is reduced and improved method of HAuCl4 synthesis packages of different thickness Au core-shell Fe2O3 @ Au nanoparticles. Measured by UV-Vis and SEM to observe the magnetic core-shell Fe2O3 @ Au nanoparticles characterization. Key words: metal composite nano-materials; spindle; Fe2O3；Fe2O3@Au  目录 1绪论 3 1.1 金属核壳纳米材料简介 3 1.1.1金属核壳纳米材料的制备 5 1.1.2金属核壳纳米材料的表征方法 9 1.2金属核壳纳米材料的应用 10 1.2.1表面增强拉曼散射的