铁粉场活化烧结初期放电击穿现象的研究.pdfVIP

I43铁粉场活化烧结初期放电击穿现象的研究 赖燕根 叶永权李小强李元元 （华南理工大学国家金属材料近净成形工程技术研究中心，广州 510640 ） 摘要：本文就羰基铁粉场活化烧结过程中的放电击穿现象进行研究。结果表明，当采用 Si N 陶瓷模具进行低压烧结， 3 4 且升温速度为 50 ℃/min 、烧结温度在 30~800 ℃范围内时，在烧结初期样品边缘会发生放电击穿，击穿孔周边呈典型 的魏氏体铸钢组织，由粗大的白色块状、针状铁素体和黑色的珠光体组成；其他区域则观察不到类似的放电组织，其 组织主要为铁素体＋条状渗碳体。放电击穿可令击穿影响区在烧结初期实现快速固结，但这种局部区域的放电对后续 烧结过程无明显影响，烧结主要通过电阻热完成。而且，过于强烈的放电会导致烧结体组织不均匀，甚至失效。 关键词：场活化烧结；放电；击穿；微观组织 Research of the discharge breakdown phenomenon in the initial stage of field activated sintering of iron powders LAI Yangen ，YE Yongquan ，LI Xiaoqiang ，LI Yuanyuan (National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials, South China University of Technology, Guangzhou 510640, China) Abstract: The discharge breakdown phenomenon observed in the field activated sintering carbonyl iron powders was studied in this paper. The result shows that the edges of the samples are broken down at the initial stage of the field activated sintering with low pressure when a Si3N4 ceramic die is used and the sintering temperature is between 30 ℃ and 800 ℃ with a heating rate of 50 ℃/min. The microstructure near to the perforation is typical cast steel, consisting of big white block, acicular ferrite and black pearlite, presenting the state of Widmanstatten structure. But the similar microstructure is not observed in the other regions of the sample, which is mainly composed of ferrite and strip cementite. Discharge breakdown can enable breakdown affected zone to consolidate rapidly in the initial stage of sintering. However, the discharge of local area has no effect on th