EBSD技术在硬质合金晶粒长大研究中的应用.pdfVIP

EBSD技术在硬质合金晶粒长大研究中的应用 刘雪梅1，宋晓艳1，赵世贤1，张久兴1，殷福星2 1．北京工业大学材料学院／新型功能材料教育部重点实验室，北京100124： 2．日本国立材料科学研究所，筑波305—0047，日本 摘要本文采用XRD、EBSD等测试手段，对WC-Co硬质合金材料的相成分和微观组织进行测试和分析， 结果表明，获得的试样具有高的致密度以及纯净的wc和co相，试样内晶粒没有择优取向；绕[1010] 轴取向角为90。的WC-WC晶界为∑2低能晶界，该种晶界大量存在且均匀分布于试样中；∑2低能晶界 与wC晶粒的长大没有直接关系。 关键词热压烧结，EBSD，WC--Co硬质合金，晶粒长大，低能晶界 中图分类号：TFl24 the incementedcarbidesEBSD of WC Analysis graingrowth by technology Liu Fuxin92 Xuemeil，SongXiaoyanl，ZhaoShixianl，ZhangJiuxin91，Yin MaterialsScienceand ofAdvancedFunctional of Materials，China 1．College Engineering,KeyLaboratory ofEducation,BeijingUniversityofTechnology，Beijing100124，P．R．China； Ministry 2．NationalInstituteforMaterials Abstract：Theconstitutionandmicrostmctureofthecementedcarbideswerecharacterizedand phase and andthe were XRDEBSD constitutionobtained analyzedby technology．Thehighdensity purephase hot methods．Themisorientationdistribution a by pressingsintering function(MDF)showspreferred boundariesas l misorientationofWC—WC 900with to 0 relationship grain respectthe[10】direction． inthe Theseboundariesarethe boundariesmaterial．ThesizeintheSPSed grain low-energy grain sample issmallerthanthatinthe thenumberfractionofthelow boundariesisnot hot-pressedsample，but energy indicatesthattheWC isnotrelatedthelow boundaries． changed．T