利用X_射线衍射法测定竹材纤维素结晶度.pdfVIP

38 8 Vol. 38 No. 8 2010 8 JOURNAL OF NORTHEAST FORESTRY UN IVERSITY Aug. 2010 X1) 杨淑敏 江泽慧 任海青 费本华 (, , 100091) 应用 X射线衍射法对毛竹发育过程中的纤维素结晶度, 以及不同造林方式和不同竹种的纤维素结 晶度 定分析, 结果表明: 毛竹材成熟过程中, 随竹龄增加纤维素结晶度的变化没有呈现明显的规律性,介于 51% ~ 5 % 之间纤维素结晶度的比例是从竹青到竹黄逐渐降低, 在竹干高度上的变化规律与竹龄有关竹龄竹干高 度和竹壁径向位置对纤维素结晶度的影响差异不显著对比两种造林方式的纤维素的结晶度, 各 个竹龄竹鞭侧芽 育苗的纤维素结晶度均小于实生苗的相应值6种竹材纤维素结晶度以孝顺竹的最大, 毛竹的最小, 介于 3% ~ 52% 之间 竹材; 纤维素结晶度; X射线衍射法 S795! S781. 1; Q 3 . 12 D eterm ination of Cellu lose C ry stallin ity of B am boo Cu lm s w ith X ray D iffrac tion Spectrum /Yang Shum in, Jiang Zehu,i Ren H aiqing, FeiBenhua( Research Institute ofW ood Industry, Ch ineseA cadem y of Forestry, Beijing 100091, P. R. China) / / Journal of Northeast Forestry University. - 2010, 38( 8). - 75~ 77 The cellu lose crystallin ity in develop ing culm s ofm oso bam boo (Phy llos tachy sp ubescens f. lu tea W en), and in culm s of different species or by different reforestation m ethodswas analysed byXray diffraction estmi ation. Result show s that the variation in cellulose crystallinity w ith age for the developingm oso bam boo is irregu lar, ranging from 51 percent to 5 per cent. The longitud inal variation in crystallin ity is related to the age, and the cellulose crystallin ity decreased from the outer to the inner parts of the culm w al.l There are no sign ificant differences bewt een cellulose crystallinity and age, cu lm height, radial position. The cellulose crystallinity of the bam boo cu lm s emerging from rh izom es is sm aller than that of the seed lings of the sam e age. The cellulose crystallin ity of six bam boo species ranges from 3 percent to 52 percent, and B am busa tex tiles show s the highest valuew hile the moso bamboo show s the low est one.