原创力文档Synthesis of PlatinCarbon XC72R Nanocomposite Using as Electrocatalyst for Direct Methanol Fuel Cells.pdfVIP
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Synthesis of PlatinCarbon XC72R Nanocomposite Using as Electrocatalyst for Direct Methanol Fuel Cells.pdf
J．Chem．Chem．Eng．6(2012)925—929
0 Lri暑 H lN为
SynthesisofPlatin／CarbonXC72R Nanocomposite
UsingasEIeCtr0CataIyStforDirectMethanoIFueICells
PhongP．T．Nguyen ，MinhH．Ngo一，Liem T．Ngo andThangC．M ．Nguyen
，．UniversityofScience，VNU-HCM,HeMCiyt
2．LacHongUniversiyt
Received：September20，2012／Accepted：October17，2012／Published：October25，2012
Abstract：Platinum／CarbonXC72R (P C)nanocompositewassynthesizedin—situbypolyolmethod．Precursorofhexahydrated
chloroplatinicacidH，PtCI6．6H2OwasreducedbyEG(ethyleneglyco1)soastoforillPtnanoparticleswhichweredepositedonthe
surfaceofcarbon．Pt／Ccompositesftreatedoruntreatedcarbon)weresynthesizedatpH ：6．5andpH= l1．TheXRDpatternofPt／C
showedpeaksassignedtothecrystallinestructureofPtandcrabon．TEM imagesshowedthatPtnanoparticlesoncarbonwereultrafine
spheresandtheparticlesobtainedsizesfrom 2to6nm whicharemostlyconcentratedonsizeof3nm ．Theelectrocatalyticactivityof
Pt／CcatalyststowardmethanoloxidationwasexaminedbyCv(cyclicvoltammetry)．Pt／treatedXC72R(pH=l1)atpotential(0．69V)
exhibitedbetterelectroactivity(628mAm／gPt)．
Keywords：Nanocompositeplatinum／carbon，electrocatalyst，DMFC(directmethanolfuelcells)，cyclicvoltammetry
1．Intr0ductiOn theirparticlesizes，distributions，andtypesofsupport．
AccordingtoSenthileta1．6【]，activatedcarbonis
Amongdifferenttypesoffuelcells，DMFC (direct
considered to be used asone ofthe bestcatalyst
methanolfuelcells)arepromisingashighlyefficient
supports．Forthepreparation ofPt／C nanocomposite，
andcleanenergysource[1]．Methanoloffersseveral
polyolmethodwasreportedasanattractiveroutesince
advantagesover hydrogen including the
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