《Miniature Flow-Through Low-Temperature Plasma Ionization Source for Ambient Ionization of Gases and Aerosols》.pptVIP

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2017-05-13 发布于浙江
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《Miniature Flow-Through Low-Temperature Plasma Ionization Source for Ambient Ionization of Gases and Aerosols》.ppt

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Figure 5. Comparison of the conventional and flow-through geometries using mass spectra from ethyl cellulose pyrolyzed in the commercial pyrolysis instrument and ionized using the miniature LTPI source and nitrogen gas in the (A) conventional and (B) flow-through LTPI configuration. 4.Conclusions Experiments suggest that the differences in the relative intensity of ions observed in the mass spectrum using the miniature LTPI source in the conventional versus flow-through configuration are due to changes in the desorption/ionization efficiency of lower mass compounds. Results show that the reproducibility of the miniature LTPI source in the flowthrough configuration is greater than the reproducibility of the miniature LTPI source in the conventional configuration. ① ② Thank you ！ * * RepReporter: Liu WeiorWei TThe Literature Reporttu re Report DateDate：2016-03-10 6-03-10 Miniature Flow-Through Low-Temperature Plasma Ionization Source for Ambient Ionization of Gases and Aerosols University of North Carolina at Chapel Hill, Department of Chemistry,USA Experimental Results and Discussions Conclusions Background 1.Background Low-temperature plasma ionization (LTPI) is a recently developed ionization technique based on a dielectric barrier discharge. LTPI has been used for a variety of applications and has been demonstrated to be a versatile ambient ionization technique, capable of generating ions from compounds in solids,solutions, gases,or aerosol particles. ① ② 2.Experimental section Materials：Ethyl cellulose and Caffeine. LTPI Power Supply Figure 1. Schematic for the power supply used to generate the lowtemperature plasma. Variable output from 0?4.25 kV with a frequency of 5 kHz. Low-Temperature Plasma Ion Source Designs. Figure 2. Schematic for the design of the miniature LTPI source. Inert gas or sample is flowed through fingertight fittings and the glass capillary to perform conventional or flow-through LTPI, respectively. A discharge is formed between the grounde