Solid-contact K+-selective electrode based on three-dimensional molybdenum sulfide nanoflowers as ion-to-electron transducer.pdfVIP

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Solid-contact K+-selective electrode based on three-dimensional molybdenum sulfide nanoflowers as ion-to-electron transducer.pdf

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Solid-contact K+-selective electrode based on three-dimensional molybdenum sulfide nanoflowers as ion-to-electron transducer.pdf

Sensors and Actuators B 234 (2016) 80–83 Contents lists available at ScienceDirect Sensors and Actuators B: Chemical journal homepage: /locate/snb Solid-contact K+-selective electrode based on three-dimensional molybdenum sul?de nano?owers as ion-to-electron transducer Xianzhong Zeng a,b, Shunyang Yu a, Qun Yuan c, Wei Qin a,? a Key Laboratory of Coastal Environmental Processes and Ecological Remediation, Yantai Institute of Coastal Zone Research (YIC), Chinese Academy of Sciences (CAS); Shandong Provincial Key Laboratory of Coastal Environmental Processes, YICCAS, Yantai, Shandong 264003, PR China b University of Chinese Academy of Sciences, Beijing 100039, PR China c College of Chemistry and Chemical Engineering, Yantai University, Yantai 264005, PR China article info Article history: Received 11 January 2016 Received in revised form 19 April 2016 Accepted 26 April 2016 Available online 27 April 2016 Keywords: MoS2 nano?owers Solid contact Ion-selective electrodes Potentiometry Potassium abstract Three-dimensional (3D) molybdenum sul?de (MoS2) nano?owers have been synthesized via a novel hydrothermal method and applied as ion-to-electron transducer for solid-contact ion-selective electrodes (SC-ISEs). The morphology and elemental composition of the prepared nanomaterials have been characterized. The performance of the developed K+-SC-ISE has been demonstrated by determining K+ in solution with a polymeric membrane containing valinomycin as the ionophore. A Nernstian slope of 55.8 mV/decade with a detection limit of 10?5.5 M can be obtained. Using the 3D ?owerlike MoS2 as solid contact, the fabricated K+-SC-ISE exhibits a smaller impedance and more stable potential response than the coated-wire electrode. In addition, the novel SC-ISE behaves well in the water layer test and shows good resistance to interferences from light, O2 and CO2. It is believed that the 3D MoS2 nano?owers can be a good alternative as solid contact in SC-ISEs. ? 2016 Elsevier B.V. All rights