New correlation for liquid hold-up of sodium citrate buffer solution in a Raschig ring packed column.pdfVIP

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New correlation for liquid hold-up of sodium citrate buffer solution in a Raschig ring packed column.pdf

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New correlation for liquid hold-up of sodium citrate buffer solution in a Raschig ring packed column

ELSEVIER Pll: SOSSO-4214(96)00016-3 Gas. Sep. Purif. Vol. 10, No. 4, pp. 199-205, 1996 Copyright 8 1996 Elsevier Science Ltd Printed in Great Britain. All rights reserved 0950-4214196 $15.00 + 0.00 New correlation for liquid hold-up of sodium citrate buffer solution in a Raschig ring packed column 1. BBgyi,= E. M6rkP and E. Bbkhssy-MohGrb aTechnical University of Budapest, Department of Chemical Engineering, 1521 Budapest, Hungary bUniversity of Horticulture and Food, Department of Food Engineering, 1118 Budapest, Menesi lit 44, Hungary Dynamic liquid hold-up was measured with an air/aqueous sodium citrate buffer solution at 20-4O”C, and an air/water system at 23”C, in a 0.1 m diameter/l m high glass column covered by a heat-isolating vacuum jacket and packed with 0.012 m nominal size ceramic Raschig rings. The superficial gas velocity range was extended to 1.2 m s-l. Experimental results of this work were compared with literature data, with different correlations and with a general equation. All expressions were found to be unacceptable for the air/buffer system and useable for the air/water system. In the case of the air/buffer solution a new correlation is recommended on the basis of our measured data and literature values. Copyright @ 1996 Elsevier Science Ltd Keywords: liquid hold-up; Raschig ring packed column; sulfur dioxide; sodium citrate buffer solution Nomenclature a ah C, ch, k CNaOH/CH,Ci D d Fi FV Surface area of packing per unit volume of packed bed (m2 mp3) Hydraulic area of packing per unit volume of packed bed (mZ mp3) Constants Concentration ratio of NaOH and citric acid (dimensionless) Diameter of the column (m) Nominal packing size (m) Film number (Fr/Re) (dimensionless) Froude number (= u2g-‘d-l) (dimensionless) Gravitational acceleration (m sp2) Dynamic liquid hold-up (ml md3) Static hold-up (m3 mb3) h, Total liquid hold-up (m3 m-3) L Liquid flow rate (m3 rnp2 h-l) Re Reynolds number (= pudq-‘