HPLC determination of berberine hydrochloride pills Niantong content.docVIP

 PAGE \* MERGEFORMAT 10 HPLC determination of berberine hydrochloride pills Niantong content Author: Pang Xiao-Xiong, SONG powder cloud, Chung Siu-Jian, XIA Han-Ming [Abstract] Objective To determine the twist in pain pills berberine hydrochloride. Methods using ion-pair chromatography, Diamonsil C18 column, acetonitrile  water (volume ratio 52:48) (per 1 000 mL plus potassium dihydrogen phosphate 3.4 g, sodium lauryl sulfate 1.7 g) as the mobile phase, flow rate of 1.0 mL * min-1, detection wavelength 265 nm, column temperature at room temperature. Results The average recovery of berberine hydrochloride 99.8%, RSD of 2.89% (n = 6). Conclusion This method can be used to twist the pain pills determination of berberine hydrochloride. [Keywords:] twist pain pill; berberine hydrochloride; ion-pair chromatography; determination Abstract: Objective To develop a method for the content determination of berberine hydrochloride in Niantongwan. Methods The analysis was performed on a Diamonsil  C18 column using acetonitrile  water (52:48, containing 3.4 g of potassium dihydrogen phosphate and 1.7 g of sodium laurylsulfate per 1 000 mL) as mobile phase. The flow rate was 1.0 mL * min-1 and the detection wavelength 265 nm.Results The average recovery for berberine hydrochloride was 99.8% with RSD 2.89% (n = 6). Conclusion The method can be used for the content determination of berberine hydrochloride in Niantongwan. Keywords:: Niantongwan; berberine hydrochloride; HPLC Niantong Pills for the Hong Kong-registered Chinese medicine set prescription preparations, from patchouli, Corydalis, magnolol, berberine and other 18 Chinese herbal medicines are made with a solution of table dampness, qi and stomach, dampness addition to full, warm in the analgesic efficacy of . Clinical for the treatment of exogenous Feng Xie, wet ride hysteresis caused by aversion to cold fever, abdominal pain, vomiting and diarrhea, dizziness, various upper and lower body pain, Kaneharu mo